GB1017463A – Process and apparatus for the continuous manufacture of polycondensation products
– Google Patents
GB1017463A – Process and apparatus for the continuous manufacture of polycondensation products
– Google Patents
Process and apparatus for the continuous manufacture of polycondensation products
Info
Publication number
GB1017463A
GB1017463A
GB45341/61A
GB4534161A
GB1017463A
GB 1017463 A
GB1017463 A
GB 1017463A
GB 45341/61 A
GB45341/61 A
GB 45341/61A
GB 4534161 A
GB4534161 A
GB 4534161A
GB 1017463 A
GB1017463 A
GB 1017463A
Authority
GB
United Kingdom
Prior art keywords
reactor
stirrer
rotation
rotating
boundary wall
Prior art date
1960-12-16
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB45341/61A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Farbwerke Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1960-12-16
Filing date
1961-12-18
Publication date
1966-01-19
1961-12-18
Application filed by Hoechst AG, Farbwerke Hoechst AG
filed
Critical
Hoechst AG
1966-01-19
Publication of GB1017463A
publication
Critical
patent/GB1017463A/en
Status
Expired
legal-status
Critical
Current
Links
Espacenet
Global Dossier
Discuss
Classifications
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
C08G63/78—Preparation processes
C08G63/785—Preparation processes characterised by the apparatus used
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F29/00—Mixers with rotating receptacles
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F29/00—Mixers with rotating receptacles
B01F29/60—Mixers with rotating receptacles rotating about a horizontal or inclined axis, e.g. drum mixers
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F29/00—Mixers with rotating receptacles
B01F29/60—Mixers with rotating receptacles rotating about a horizontal or inclined axis, e.g. drum mixers
B01F29/63—Mixers with rotating receptacles rotating about a horizontal or inclined axis, e.g. drum mixers with fixed bars, i.e. stationary, or fixed on the receptacle
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F33/00—Other mixers; Mixing plants; Combinations of mixers
B01F33/25—Mixers with loose mixing elements, e.g. loose balls in a receptacle
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
B01F35/90—Heating or cooling systems
B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J19/18—Stationary reactors having moving elements inside
B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J19/28—Moving reactors, e.g. rotary drums
B—PERFORMING OPERATIONS; TRANSPORTING
B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
B02C17/04—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container
B02C17/06—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with unperforated container with several compartments
B—PERFORMING OPERATIONS; TRANSPORTING
B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
B02C17/00—Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
B02C17/18—Details
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
C08G69/04—Preparatory processes
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
B01F27/05—Stirrers
B01F27/11—Stirrers characterised by the configuration of the stirrers
B01F27/115—Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J2219/00049—Controlling or regulating processes
B01J2219/00051—Controlling the temperature
B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J2219/00049—Controlling or regulating processes
B01J2219/00051—Controlling the temperature
B01J2219/00132—Controlling the temperature using electric heating or cooling elements
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J2219/00049—Controlling or regulating processes
B01J2219/00051—Controlling the temperature
B01J2219/0015—Controlling the temperature by thermal insulation means
B01J2219/00155—Controlling the temperature by thermal insulation means using insulating materials or refractories
B—PERFORMING OPERATIONS; TRANSPORTING
B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
B01J2219/18—Details relating to the spatial orientation of the reactor
B01J2219/187—Details relating to the spatial orientation of the reactor inclined at an angle to the horizontal or to the vertical plane
Abstract
A polycondensable mixture is reacted in a continuous process by feeding it into a reactor having a stirrer or boundary wall in rotation or rotary oscillation about a horizontal or inclined axis through which flows a polymer containing liquid the stirrer or boundary wall being heated only at a point which is in contact with the liquid. The polycondensate may be a saturated linear or unsaturated polyester, a polyether or a polyamide. The reactor may be conical or cylindrical in shape and may contain annular partitions at right angles to the rotating wall. It may be 1/4 -\ba1/3 full. Additional agitation may be provided by (a) metal balls, (b) an axially mounted agitator in the form of a disc, blade or screw which is stationary or rotating at a different speed to the reactor, (c) baffle plates or (d) inclination of the reactor. Heat may be supplied by electrical means or by immersing 1/4 or 1/3 of the reactor in a hot fluid bath. The electrical heating means may comprise a number of elements either arranged as blades of a stirrer, or fixed to the outside of the rotating boundary wall coupled to equipment which allows them to be switched on and off in rotation. The reaction may be carried out in a number of stages each stage being a process as previously described but the speed of rotation and degree of heating decreasing in the direction in which the polymer flows. Several embodiments of the invention are illustrated. In an example polyethylene terephthalate is prepared using a zinc acetate catalyst.
GB45341/61A
1960-12-16
1961-12-18
Process and apparatus for the continuous manufacture of polycondensation products
Expired
GB1017463A
(en)
Applications Claiming Priority (2)
Application Number
Priority Date
Filing Date
Title
DEF32776A
DE1207349B
(en)
1960-12-16
1960-12-16
Device for the continuous production of polycondensates
DEF0033120
1961-02-03
Publications (1)
Publication Number
Publication Date
GB1017463A
true
GB1017463A
(en)
1966-01-19
Family
ID=25974847
Family Applications (1)
Application Number
Title
Priority Date
Filing Date
GB45341/61A
Expired
GB1017463A
(en)
1960-12-16
1961-12-18
Process and apparatus for the continuous manufacture of polycondensation products
Country Status (5)
Country
Link
US
(1)
US3220804A
(en)
BE
(1)
BE611659A
(en)
DE
(1)
DE1207349B
(en)
GB
(1)
GB1017463A
(en)
NL
(1)
NL272388A
(en)
Cited By (2)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US3544522A
(en)
*
1961-07-24
1970-12-01
Inventa Ag
Continuous manufacture of polymers
WO1990005157A1
(en)
*
1988-11-01
1990-05-17
Boehringer Ingelheim Kg
Continuous process for manufacturing resorbable polyesters and their use
Families Citing this family (19)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US3457291A
(en)
*
1965-04-01
1969-07-22
Union Carbide Corp
Production of isocyanates
CH444126A
(en)
*
1965-09-08
1967-09-30
Inventa Ag
Device for the continuous implementation of chemical reactions in viscous liquids
US3617225A
(en)
*
1967-06-22
1971-11-02
Vickers Zimmer Ag
Polycondensation apparatus
US4060587A
(en)
*
1975-06-30
1977-11-29
National Lime Association
Gaseous and liquid reactant treatment
DE2609430C3
(en)
*
1976-03-06
1981-04-02
Skw Trostberg Ag, 8223 Trostberg
Apparatus for the production of vanadium pentoxide
DE3514367A1
(en)
*
1985-04-20
1986-10-23
Basf Ag, 6700 Ludwigshafen
DEVICE FOR SOLID BED POLYMERIZATION OF MONOMERS
US5047349A
(en)
*
1986-10-07
1991-09-10
Bedminster Bioconversion Corporation
Multi-compartment rotating drum apparatus for the fermentation of natural organic material
EP0495133A1
(en)
*
1991-01-12
1992-07-22
Pfaudler Werke GmbH
Corrosion protected stirrer with removable agitating vane unit
EP1114141A4
(en)
*
1998-09-18
2004-04-14
Paul E Kerouac
In vessel composting process and apparatus
AU2411900A
(en)
1999-01-12
2000-08-01
Paul Kerouac
In vessel composting process and apparatus
ITTO20020714A1
(en)
*
2002-08-09
2004-02-10
Giuliano Cavaglia
CONTINUOUS POLYMERIZATION PROCEDURE FOR
DE102004031837A1
(en)
*
2004-06-30
2006-01-19
Bühler AG
Reactor for (especially thermo-chemical) treatment of bulk goods always has its outlet above a predetermined minimum height above the deepest part of the mixing chamber
DE102004034708B4
(en)
*
2004-07-17
2008-04-10
Lurgi Zimmer Gmbh
Process for the batch production of polymers by melt condensation
ITTO20070084A1
(en)
*
2007-02-06
2008-08-07
K & E Srl
RADIAL MIXING DEVICES FOR ROLLING INCLINED REACTORS.
CN101402062B
(en)
*
2008-11-14
2010-11-10
昆明理工大学
Vertical coaxial anticentripetal grinder
US20100139490A1
(en)
*
2008-12-08
2010-06-10
General Electric Company
Method and system for centrifugal resin degassing
CN103833996B
(en)
*
2013-12-31
2016-02-24
常州华日新材有限公司
Resin production plant
US10293314B2
(en)
*
2016-08-02
2019-05-21
Dimitri Spiro Karatsinides
Temperature controlled rotating apparatus
DE102018105130A1
(en)
*
2018-03-06
2019-09-12
Torsten Heitmann
Apparatus and method for agitation of liquids or bulk material
Family Cites Families (10)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US640283A
(en)
*
1899-03-04
1900-01-02
Francis E Hatch
Electric furnace.
US706334A
(en)
*
1902-02-03
1902-08-05
George Moore
Apparatus for leaching ores, &c.
US1004509A
(en)
*
1910-02-23
1911-09-26
American Cyanamid Co
Method of making cyanamid
US1118775A
(en)
*
1912-10-24
1914-11-24
John Hyde
Pulverizer.
US1593879A
(en)
*
1923-04-21
1926-07-27
John J Naugle
Electric furnace
US1862557A
(en)
*
1926-05-14
1932-06-14
Nat Aniline & Chem Co Inc
Ball mill
US1834693A
(en)
*
1926-12-04
1931-12-01
Frischer Hermann
Means of promoting chemical reactions
DE481744C
(en)
*
1927-01-04
1929-09-02
Adolf Kaempf Dr Ing
Device for carrying out physical and chemical reactions
US2758915A
(en)
*
1953-07-02
1956-08-14
Du Pont
Apparatus for continuous polymerization
US2964391A
(en)
*
1956-12-19
1960-12-13
Ici Ltd
Manufacture of synthetic linear polymers
0
NL
NL272388D
patent/NL272388A/xx
unknown
1960
1960-12-16
DE
DEF32776A
patent/DE1207349B/en
active
Pending
1961
1961-12-12
US
US158816A
patent/US3220804A/en
not_active
Expired – Lifetime
1961-12-18
GB
GB45341/61A
patent/GB1017463A/en
not_active
Expired
1961-12-18
BE
BE611659A
patent/BE611659A/en
unknown
Cited By (3)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US3544522A
(en)
*
1961-07-24
1970-12-01
Inventa Ag
Continuous manufacture of polymers
WO1990005157A1
(en)
*
1988-11-01
1990-05-17
Boehringer Ingelheim Kg
Continuous process for manufacturing resorbable polyesters and their use
EP0372221A1
(en)
*
1988-11-01
1990-06-13
Boehringer Ingelheim Kg
Continuous process for the preparation of resorbable polyesters, and their use
Also Published As
Publication number
Publication date
US3220804A
(en)
1965-11-30
BE611659A
(en)
1962-06-18
NL272388A
(en)
DE1207349B
(en)
1965-12-23
Similar Documents
Publication
Publication Date
Title
GB1017463A
(en)
1966-01-19
Process and apparatus for the continuous manufacture of polycondensation products
EP1152824B8
(en)
2003-04-09
Rotating surface of revolution reactor with temperature control mechanisms
US3563710A
(en)
1971-02-16
Polymerization apparatus
US3591344A
(en)
1971-07-06
Device for continuous polycondensation
GB1032405A
(en)
1966-06-08
Process and apparatus for the continuous preparation of bis-2-hydroxyethyl phthalates
US3499873A
(en)
1970-03-10
Preparation of polyethylene terephthalate by means of free falling films
US3528782A
(en)
1970-09-15
Polycondensation reactor
GB1089397A
(en)
1967-11-01
Apparatus comprising a stirred vessel for conducting processes
US4728731A
(en)
1988-03-01
Reactor and its use in polysaccharide ether production
US3787481A
(en)
1974-01-22
Method for the continuous performance of esterification under thermal conditions
US3498754A
(en)
1970-03-03
Continuous polycondensation apparatus
GB1343447A
(en)
1974-01-10
Gas-liquid contact reaction
US3118739A
(en)
1964-01-21
Polymer finisher apparatus
CN105836466B
(en)
2018-08-14
The anti-tossed device of medicinal material in Chinese medicine microwave drying process
US1181973A
(en)
1916-05-02
Mixing apparatus.
US3545520A
(en)
1970-12-08
Apparatus for removing substances and fractions from polymers
ES2013581A4
(en)
1990-05-16
INSTALLATION AND PROCEDURE TO TREAT DESICTION OF ORGANIC WASTE
US3870475A
(en)
1975-03-11
Apparatus for the continuous performance of chemical processes, more particulary esterification, and/or transesterification and polycondensation processes
US3545938A
(en)
1970-12-08
Apparatus for producing and processing viscous materials
GB1369933A
(en)
1974-10-09
Preparation of polymers
US3446772A
(en)
1969-05-27
Process for preparing high molecular weight polyalkylene terephthalates by intimately mixing a molten stream of low molecular weight polyalkylene terephthalate with a melt of higher molecular weight polyalkylene terephthalate
US3510267A
(en)
1970-05-05
Polycondensation reactor
FR2019344A1
(en)
1970-07-03
Mixer and agitator
ES367710A1
(en)
1971-04-16
Improvements in the construction of devices for the policondensation of a prepolimero. (Machine-translation by Google Translate, not legally binding)
JPH03239727A
(en)
1991-10-25
Apparatus for continuously agitating viscous substance
None