GB1113722A

GB1113722A – Aerobically polymerisable compositions
– Google Patents

GB1113722A – Aerobically polymerisable compositions
– Google Patents
Aerobically polymerisable compositions

Info

Publication number
GB1113722A

GB1113722A
GB20054/65A
GB2005465A
GB1113722A
GB 1113722 A
GB1113722 A
GB 1113722A
GB 20054/65 A
GB20054/65 A
GB 20054/65A
GB 2005465 A
GB2005465 A
GB 2005465A
GB 1113722 A
GB1113722 A
GB 1113722A
Authority
GB
United Kingdom
Prior art keywords
compositions
meth
acrylate
monomer
composition
Prior art date
1964-05-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB20054/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

3M Co

Original Assignee
Minnesota Mining and Manufacturing Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1964-05-21
Filing date
1965-05-12
Publication date
1968-05-15

1965-05-12
Application filed by Minnesota Mining and Manufacturing Co
filed
Critical
Minnesota Mining and Manufacturing Co

1968-05-15
Publication of GB1113722A
publication
Critical
patent/GB1113722A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR

C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES

C09J4/00—Adhesives based on organic non-macromolecular compounds having at least one polymerisable carbon-to-carbon unsaturated bond ; adhesives, based on monomers of macromolecular compounds of groups C09J183/00 – C09J183/16

A—HUMAN NECESSITIES

A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE

A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES

A61K6/00—Preparations for dentistry

A61K6/80—Preparations for artificial teeth, for filling teeth or for capping teeth

A61K6/884—Preparations for artificial teeth, for filling teeth or for capping teeth comprising natural or synthetic resins

A61K6/887—Compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds

Abstract

Compositions which are aerobically polymerizable in the presence of a free radical catalyst comprise one or more mono- and/or bisacrylate or methacrylate monomers and 0.05-6% by weight of the monomer(s) of a triarylborane complex of the formula R3B-Am in which R represents an aryl radical of 6-12 carbon atoms and Am represents sodium hydroxide, ammonia, benzene or an amine. The radical R is preferably free from hydroxyl, carboxyl and amino groups but may contain substituents such as halo, alkyl and alkoxy groups. The (meth)acrylate monomer is one which normally polymerizes only with difficulty with a free radical catalyst unless oxygen is almost completely absent; suitable esters are alkyl, allyl and fusel oil (meth)acrylates, the bisesters of glycols and bisphenols, and the bisester condensation products of phenols and glycidyl(meth)acrylate (which may contain additional ethylenic unsaturation). The composition may also include an oxirane-type monomer, e.g. glycidyl acrylate or methacrylate or a diluent monomer such as phenyl acrylate, hydroxyethyl methacrylate or acrylonitrile. A free base may also be included as a co-catalyst component, e.g. dimethyl-p-toluidine, tri-nbutylamine, diethylenetriamine, N-methylpiperidine, N-methylmorpholine, 2,5-dimethylpiperazine or 1,2,4-trimethylpiperazine. Other optional components include solvents, fillers (e.g. silica, alumina or synthetic fluorapatite), pigments, dyes and plasticizers. To effect polymerization a free radical catalyst is added, e.g. benzoyl peroxide, methyl ethyl ketone peroxide, t-butyl hydroperoxide or azobisisobutyronitrile, and the composition is then activated by heating or acidifying, e.g. with an inorganic or organic acid; the latter is preferably a compound which will copolymerize with the (meth)acrylate monomer, e.g. acrylic, methacrylic, maleic or citraconic acid. The compositions may be stored as multi-component kit, each component containing some of the ingredients of the composition in stable form. The compositions are suitable for coating, moulding, potting, embedding or sealing and, particularly, for use as a vehicle in dental filling compositions, as described in Specification 1,113,723.

GB20054/65A
1964-05-21
1965-05-12
Aerobically polymerisable compositions

Expired

GB1113722A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US36927764A

1964-05-21
1964-05-21

Publications (1)

Publication Number
Publication Date

GB1113722A
true

GB1113722A
(en)

1968-05-15

Family
ID=23454812
Family Applications (2)

Application Number
Title
Priority Date
Filing Date

GB20054/65A
Expired

GB1113722A
(en)

1964-05-21
1965-05-12
Aerobically polymerisable compositions

GB58597/67A
Expired

GB1113723A
(en)

1964-05-21
1965-05-12
Dental filling material

Family Applications After (1)

Application Number
Title
Priority Date
Filing Date

GB58597/67A
Expired

GB1113723A
(en)

1964-05-21
1965-05-12
Dental filling material

Country Status (6)

Country
Link

JP
(1)

JPS4827735B1
(en)

CH
(2)

CH471165A
(en)

DE
(1)

DE1570971A1
(en)

FR
(1)

FR1458180A
(en)

GB
(2)

GB1113722A
(en)

SE
(1)

SE349236B
(en)

Cited By (22)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4515724A
(en)

*

1982-03-01
1985-05-07
Henkel Kommanditgesellschaft Auf Aktien
Boron alkyl compounds and processes for their manufacture and use

US4638092A
(en)

*

1982-01-21
1987-01-20
Henkel Kommanditgesellschaft Auf Aktien
New organic boron polymers and their use

US4676858A
(en)

*

1982-03-01
1987-06-30
Henkel Kommanditgesellschaft Auf Aktien
Organoboron containing mixtures and their manufacture and use

US5539070A
(en)

*

1994-02-22
1996-07-23
Minnesota Mining And Manufacturing Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US5616796A
(en)

*

1995-04-14
1997-04-01
Minnesota Mining And Manufacturing Company
Organoborane polyamine complexes and adhesive composition made therewith

US5621143A
(en)

*

1995-04-14
1997-04-15
Minnesota Mining And Manufacturing Company
Organoborane polyoxyalkylenepolyamine complexes and adhesive compositions made therewith

US5686544A
(en)

*

1995-08-11
1997-11-11
Minnesota Mining And Manufacturing Company
Organoborane polyamine complex initiator systems and polymerizable compositions made therewith

US5691065A
(en)

*

1995-02-22
1997-11-25
Minnesota Mining And Manufacturing Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US5872197A
(en)

*

1995-08-11
1999-02-16
Minnesota Mining & Manufacturing Company
Initiator system and adhesive composition made therewith

US5883208A
(en)

*

1995-11-07
1999-03-16
Minnesota Mining And Manufacutring Company
Initiator system and adhesive composition made therewith

US5935711A
(en)

*

1996-10-23
1999-08-10
3M Innovative Properties Company
Organoborane amine complex initiator systems and polymerizable compositions made therewith

US5952409A
(en)

1996-01-31
1999-09-14
3M Innovative Properties Company
Compositions and methods for imparting stain resistance and stain resistant articles

EP0985684A2
(en)

*

1998-09-10
2000-03-15
MERCK PATENT GmbH
New reactive systems of polymerisable monomers containing peroxyds and stabilised alkyl boron compounds

WO2000066069A1
(en)

*

1999-04-29
2000-11-09
3M Espe Ag
Dental materials

US6252023B1
(en)

1999-03-19
2001-06-26
3M Innovative Properties Company
Organoborane amine complex inatator systems and polymerizable compositions made therewith

DE19959514C1
(en)

*

1999-12-09
2001-08-30
Heraeus Kulzer Gmbh & Co Kg

Dental investment material

US6383655B1
(en)

1998-06-12
2002-05-07
3M Innovative Properties Company
Low odor polymerizable compositions useful for bonding low surface energy substrates

US6479602B1
(en)

2000-03-15
2002-11-12
3M Innovative Properties
Polymerization initiator systems and bonding compositions comprising vinyl aromatic compounds

US6630555B2
(en)

2001-11-06
2003-10-07
Lord Corporation
Internally blocked organoborate initiators and adhesives therefrom

US6799966B1
(en)

1999-03-04
2004-10-05
3M Innovative Properties Company
Fluoropolymeric orthodontic article

US6812308B2
(en)

2000-11-21
2004-11-02
3M Innovative Properties Company
Initiator systems and adhesive compositions made therewith

WO2006026065A2
(en)

*

2004-08-30
2006-03-09
Ultradent Products, Inc.
Gas releasing sealing and filling compositions

Families Citing this family (4)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

JPS5137092B2
(en)

*

1972-04-28
1976-10-13

IE37703B1
(en)

*

1972-11-16
1977-09-28
Loctite Ltd
Protective adhesive-carrying tape

CA1117685A
(en)

*

1976-11-15
1982-02-02
Narayanan Madhavan
One paste polymeric dental restorative composition

JP6883300B1
(en)

*

2020-03-04
2021-06-09
株式会社球体研究所

Negative thermal expansion fine particles and their manufacturing method

1965

1965-05-12
GB
GB20054/65A
patent/GB1113722A/en
not_active
Expired

1965-05-12
GB
GB58597/67A
patent/GB1113723A/en
not_active
Expired

1965-05-17
DE
DE19651570971
patent/DE1570971A1/en
active
Pending

1965-05-20
FR
FR17704A
patent/FR1458180A/en
not_active
Expired

1965-05-20
CH
CH14668A
patent/CH471165A/en
not_active
IP Right Cessation

1965-05-20
CH
CH707665A
patent/CH475762A/en
not_active
IP Right Cessation

1965-05-21
JP
JP40029655A
patent/JPS4827735B1/ja
active
Pending

1965-05-21
SE
SE06654/65A
patent/SE349236B/xx
unknown

Cited By (42)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4638092A
(en)

*

1982-01-21
1987-01-20
Henkel Kommanditgesellschaft Auf Aktien
New organic boron polymers and their use

US4515724A
(en)

*

1982-03-01
1985-05-07
Henkel Kommanditgesellschaft Auf Aktien
Boron alkyl compounds and processes for their manufacture and use

US4676858A
(en)

*

1982-03-01
1987-06-30
Henkel Kommanditgesellschaft Auf Aktien
Organoboron containing mixtures and their manufacture and use

US5539070A
(en)

*

1994-02-22
1996-07-23
Minnesota Mining And Manufacturing Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US6248846B1
(en)

1994-02-22
2001-06-19
3M Innovative Properties Company
Polymerizable compositions comprising organoborane amine complexes

US6284381B1
(en)

*

1994-02-22
2001-09-04
3M Innovative Properties Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US5690780A
(en)

*

1995-02-22
1997-11-25
Minnesota Mining And Manufacturing Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US5691065A
(en)

*

1995-02-22
1997-11-25
Minnesota Mining And Manufacturing Company
Polymerizable compositions made with polymerization initiator systems based on organoborane amine complexes

US5621143A
(en)

*

1995-04-14
1997-04-15
Minnesota Mining And Manufacturing Company
Organoborane polyoxyalkylenepolyamine complexes and adhesive compositions made therewith

US5616796A
(en)

*

1995-04-14
1997-04-01
Minnesota Mining And Manufacturing Company
Organoborane polyamine complexes and adhesive composition made therewith

US5681910A
(en)

*

1995-04-14
1997-10-28
Minnesota Mining And Manufacturing Company
Organoborane polyoxyalkylenepolyamine complexes and adhsesive compositions made therewith

US5718977A
(en)

*

1995-04-14
1998-02-17
Minnesota Mining And Manufacturing Company
Organoborane polyoxyalkylenepolyamine complexes and adhesive compositions made therewith

US5795657A
(en)

*

1995-04-14
1998-08-18
Minnesota Mining And Manufaturing Company
Organoborane polyamine complexes and adhesive compositions made therewith

US5684102A
(en)

*

1995-04-14
1997-11-04
Minnesota Mining And Manufacturing Company
Organoborane polyamine complexes and adhesive compositions made therewith

US5872197A
(en)

*

1995-08-11
1999-02-16
Minnesota Mining & Manufacturing Company
Initiator system and adhesive composition made therewith

US5686544A
(en)

*

1995-08-11
1997-11-11
Minnesota Mining And Manufacturing Company
Organoborane polyamine complex initiator systems and polymerizable compositions made therewith

US6093778A
(en)

*

1995-08-11
2000-07-25
3M Innovative Properties Company
Organoborane polyamine complex initiator systems and polymerizable compositions made therewith

US5990036A
(en)

*

1995-08-11
1999-11-23
3M Innovative Properties Company
Initiator system and adhesive composition made therewith

US5994484A
(en)

*

1995-08-11
1999-11-30
3M Innovative Properties Company
Organoborane polyamine complex initiator systems and polymerizable compositions made therewith

US6008308A
(en)

*

1995-08-11
1999-12-28
3M Innovative Properties Company
Organoborane polyamine complex initiator systems and polymerizable compositions made therewith

US6027813A
(en)

*

1995-11-07
2000-02-22
3M Innovative Properties Company
Initiator system and adhesive composition made therewith

US5883208A
(en)

*

1995-11-07
1999-03-16
Minnesota Mining And Manufacutring Company
Initiator system and adhesive composition made therewith

US5952409A
(en)

1996-01-31
1999-09-14
3M Innovative Properties Company
Compositions and methods for imparting stain resistance and stain resistant articles

US5935711A
(en)

*

1996-10-23
1999-08-10
3M Innovative Properties Company
Organoborane amine complex initiator systems and polymerizable compositions made therewith

US7189303B2
(en)

1998-06-12
2007-03-13
3M Innovative Properties Company
Initiator systems and adhesive compositions made therewith

US6383655B1
(en)

1998-06-12
2002-05-07
3M Innovative Properties Company
Low odor polymerizable compositions useful for bonding low surface energy substrates

EP0985684A2
(en)

*

1998-09-10
2000-03-15
MERCK PATENT GmbH
New reactive systems of polymerisable monomers containing peroxyds and stabilised alkyl boron compounds

EP0985684A3
(en)

*

1998-09-10
2000-04-26
MERCK PATENT GmbH
New reactive systems of polymerisable monomers containing peroxyds and stabilised alkyl boron compounds

US6799966B1
(en)

1999-03-04
2004-10-05
3M Innovative Properties Company
Fluoropolymeric orthodontic article

US6252023B1
(en)

1999-03-19
2001-06-26
3M Innovative Properties Company
Organoborane amine complex inatator systems and polymerizable compositions made therewith

US6384165B1
(en)

1999-03-19
2002-05-07
3M Innovative Properties Co.
Organoborane amine complex initiator systems and polymerizable compositions made therewith

WO2000066069A1
(en)

*

1999-04-29
2000-11-09
3M Espe Ag
Dental materials

US6652281B1
(en)

1999-04-29
2003-11-25
3M Espe Ag
Dental materials

US6575750B2
(en)

1999-12-09
2003-06-10
Heraeus Kulzer Gmbh & Co. Kg
Dental embedding material, dental kit and method for making a prosthesis

DE19959514C1
(en)

*

1999-12-09
2001-08-30
Heraeus Kulzer Gmbh & Co Kg

Dental investment material

US6479602B1
(en)

2000-03-15
2002-11-12
3M Innovative Properties
Polymerization initiator systems and bonding compositions comprising vinyl aromatic compounds

US6812308B2
(en)

2000-11-21
2004-11-02
3M Innovative Properties Company
Initiator systems and adhesive compositions made therewith

US6841635B2
(en)

2001-11-06
2005-01-11
Lord Corporation
Internally blocked organoborate initiators and adhesives therefrom

US6630555B2
(en)

2001-11-06
2003-10-07
Lord Corporation
Internally blocked organoborate initiators and adhesives therefrom

WO2006026065A2
(en)

*

2004-08-30
2006-03-09
Ultradent Products, Inc.
Gas releasing sealing and filling compositions

WO2006026065A3
(en)

*

2004-08-30
2006-10-05
Ultradent Products Inc
Gas releasing sealing and filling compositions

US7173075B2
(en)

2004-08-30
2007-02-06
Ultradent Products, Inc.
Gas releasing sealing and filling compositions

Also Published As

Publication number
Publication date

GB1113723A
(en)

1968-05-15

FR1458180A
(en)

1966-11-10

JPS4827735B1
(en)

1973-08-25

DE1570971A1
(en)

1970-09-24

SE349236B
(en)

1972-09-25

CH475762A
(en)

1969-07-31

CH471165A
(en)

1969-04-15

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