GB1360328A

GB1360328A – Purification process for a acetic acid
– Google Patents

GB1360328A – Purification process for a acetic acid
– Google Patents
Purification process for a acetic acid

Info

Publication number
GB1360328A

GB1360328A
GB5322172A
GB5322172A
GB1360328A
GB 1360328 A
GB1360328 A
GB 1360328A
GB 5322172 A
GB5322172 A
GB 5322172A
GB 5322172 A
GB5322172 A
GB 5322172A
GB 1360328 A
GB1360328 A
GB 1360328A
Authority
GB
United Kingdom
Prior art keywords
acetic acid
iodine
acid
nov
purified
Prior art date
1971-11-19
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB5322172A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Monsanto Co

Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1971-11-19
Filing date
1972-11-17
Publication date
1974-07-17

1972-11-17
Application filed by Monsanto Co
filed
Critical
Monsanto Co

1974-07-17
Publication of GB1360328A
publication
Critical
patent/GB1360328A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C07—ORGANIC CHEMISTRY

C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS

C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides

C07C51/42—Separation; Purification; Stabilisation; Use of additives

C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation

C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation

C—CHEMISTRY; METALLURGY

C07—ORGANIC CHEMISTRY

C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS

C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides

C07C51/42—Separation; Purification; Stabilisation; Use of additives

C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Abstract

1360328 Acetic acid MONSANTO CO 17 Nov 1972 [19 Nov 1971] 53221/72 Heading C2C Acetic acid containing iodine or iodine containing impurities is purified by distilling in the presence of an alkali or alkaline earth metal oxide, hydroxide, carbonate, bicarbonate or salt of a weak organic acid or if free iodine is present, hypophosphorous acid, The process is preferably carried out in two columns, to the first of which the acid and agent are introduced intermediate, the overhead product is introduced intermedaite to the second column and the purified acetic acid removed from the lower half thereof. Examples describe the purification of crude by the carbonylation of methanol in the presence of rhodium and an iodine component with carbon monoxide. Potassium acetate is the preferred agent.

GB5322172A
1971-11-19
1972-11-17
Purification process for a acetic acid

Expired

GB1360328A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US20055371A

1971-11-19
1971-11-19

Publications (1)

Publication Number
Publication Date

GB1360328A
true

GB1360328A
(en)

1974-07-17

Family
ID=22742196
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB5322172A
Expired

GB1360328A
(en)

1971-11-19
1972-11-17
Purification process for a acetic acid

Country Status (9)

Country
Link

US
(1)

US3772156A
(en)

JP
(1)

JPS5755695B2
(en)

BE
(1)

BE791577A
(en)

CA
(1)

CA979842A
(en)

DE
(1)

DE2256510C2
(en)

FR
(1)

FR2160615B1
(en)

GB
(1)

GB1360328A
(en)

NL
(1)

NL174545C
(en)

SU
(1)

SU598556A3
(en)

Cited By (1)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US5387713A
(en)

*

1991-01-05
1995-02-07
Bp Chemicals Limited
Process for purification of carboxylic acids

Families Citing this family (32)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4029553A
(en)

*

1975-07-28
1977-06-14
Monsanto Company
Purification of acetic acid streams by distillation

US4039395A
(en)

*

1975-08-11
1977-08-02
Monsanto Company
Purification of acetic acid

US4039428A
(en)

*

1976-01-02
1977-08-02
Monsanto Company
Purification of propionic acid

US4153806A
(en)

*

1977-10-11
1979-05-08
Halcon Research And Development Corp.
Recovery of vicinal glycol esters by plural stage distillation

US4246195A
(en)

*

1978-10-06
1981-01-20
Halcon Research And Development Corporation
Purification of carbonylation products

US4241219A
(en)

*

1979-07-30
1980-12-23
Halcon Research And Development Corp.
Treatment of carbonylation effluent

DE3329781A1
(en)

*

1983-08-18
1985-02-28
Hoechst Ag, 6230 Frankfurt

METHOD FOR SEPARATING IODINE AND ITS COMPOUNDS FROM CARBONYLATION PRODUCTS OBTAINED FROM CARBONYLATING DIMETHYL ETHER, METHYL ACETATE OR METHANOL

US4599472A
(en)

*

1985-06-27
1986-07-08
Phillips Petroleum Company
Purification of iodine-containing mixtures and compositions useful therefor

US4683033A
(en)

*

1985-06-27
1987-07-28
Phillips Petroleum Company
Purification of iodine-containing mixtures and compositions useful therefor

GB8822661D0
(en)

*

1988-09-27
1988-11-02
Bp Chem Int Ltd
Removal of iodine/iodide impurities

US5237097A
(en)

*

1990-02-09
1993-08-17
Quantum Chemical Corporation
Catalytic carbonylation process

GB9120902D0
(en)

*

1991-10-02
1991-11-13
Bp Chem Int Ltd
Purification process

DE4140082A1
(en)

*

1991-12-05
1993-06-09
Hoechst Ag, 6230 Frankfurt, De

METHOD FOR PURIFYING WASTE ACID ACID

DE4327011A1
(en)

*

1993-08-12
1995-02-16
Hoechst Ag

Process for the removal of aldehydes and acetals from technically produced acetic acid

TW330200B
(en)

*

1995-09-29
1998-04-21
Showa Denko Kk
Process for purifying acetic acid

GB9626324D0
(en)

*

1996-12-19
1997-02-05
Bp Chem Int Ltd
Process

US6552221B1
(en)

1998-12-18
2003-04-22
Millenium Petrochemicals, Inc.
Process control for acetic acid manufacture

EP1114814A3
(en)

*

1999-12-29
2003-01-22
Haldor Topsoe A/S
Method for the reduction of iodine compounds from a process stream

JP4732743B2
(en)

*

2004-12-06
2011-07-27
ダイセル化学工業株式会社

Distillation method

EP2657220B1
(en)

2010-12-24
2016-08-31
Daicel Corporation
Acetic acid production method

CN104045548B
(en)

*

2013-03-14
2016-08-10
中国石油化工股份有限公司
A kind of remove the method for Trace Iodine in acetic acid

WO2016054608A1
(en)

2014-10-02
2016-04-07
Celanese International Corporation
Process for producing acetic acid

CN107207392B
(en)

2015-01-30
2021-06-08
国际人造丝公司
Process for producing acetic acid

US9487464B2
(en)

2015-01-30
2016-11-08
Celanese International Corporation
Processes for producing acetic acid

RS59401B1
(en)

2015-01-30
2019-11-29
Celanese Int Corp
Processes for producing acetic acid

US9561994B2
(en)

2015-01-30
2017-02-07
Celanese International Corporation
Processes for producing acetic acid

US9505696B2
(en)

2015-02-04
2016-11-29
Celanese International Corporation
Process to control HI concentration in residuum stream

US9512056B2
(en)

2015-02-04
2016-12-06
Celanese International Corporation
Process to control HI concentration in residuum stream

US10413840B2
(en)

2015-02-04
2019-09-17
Celanese International Coporation
Process to control HI concentration in residuum stream

US9957216B2
(en)

2015-11-13
2018-05-01
Celanese International Corporation
Processes for producing acetic acid

US10428004B2
(en)

2017-01-18
2019-10-01
Daicel Corporation
Method for producing acetic acid

JP6693959B2
(en)

*

2017-01-18
2020-05-13
株式会社ダイセル

Method for producing acetic acid

Family Cites Families (7)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US2384374A
(en)

*

1945-09-04

Recovery of acetic acid in purified

US2900413A
(en)

*

1956-03-12
1959-08-18
Celanese Corp
Purification of lower aliphatic acids

US3084109A
(en)

*

1958-04-03
1963-04-02
Ici Ltd
Recovery of monocarboxylic acids

US3196176A
(en)

*

1962-03-07
1965-07-20
Celanese Corp
Purification of acetic acid

US3490997A
(en)

*

1965-01-07
1970-01-20
Standard Oil Co
Dehydration of wet lower aliphatic monocarboxylic acid by distillation with alkali metal ions present

US3709795A
(en)

*

1970-02-02
1973-01-09
Monsanto Co
Purification of carboxylic acids by chemical treatment and distillation

GB1294432A
(en)

*

1970-04-23
1972-10-25
Monsanto Co
Purification of carboxylic acid streams

0

BE
BE791577D
patent/BE791577A/en
not_active
IP Right Cessation

1971

1971-11-19
US
US00200553A
patent/US3772156A/en
not_active
Expired – Lifetime

1972

1972-11-14
SU
SU721847388A
patent/SU598556A3/en
active

1972-11-15
NL
NLAANVRAGE7215472,A
patent/NL174545C/en
not_active
IP Right Cessation

1972-11-17
FR
FR7240945A
patent/FR2160615B1/fr
not_active
Expired

1972-11-17
GB
GB5322172A
patent/GB1360328A/en
not_active
Expired

1972-11-17
CA
CA156,901A
patent/CA979842A/en
not_active
Expired

1972-11-17
DE
DE2256510A
patent/DE2256510C2/en
not_active
Expired

1972-11-17
JP
JP47114862A
patent/JPS5755695B2/ja
not_active
Expired

Cited By (1)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US5387713A
(en)

*

1991-01-05
1995-02-07
Bp Chemicals Limited
Process for purification of carboxylic acids

Also Published As

Publication number
Publication date

JPS4861414A
(en)

1973-08-28

DE2256510A1
(en)

1973-05-30

US3772156A
(en)

1973-11-13

BE791577A
(en)

1973-05-17

SU598556A3
(en)

1978-03-15

NL7215472A
(en)

1973-05-22

AU4900272A
(en)

1974-05-23

FR2160615A1
(en)

1973-06-29

DE2256510C2
(en)

1982-05-06

NL174545C
(en)

1984-07-02

FR2160615B1
(en)

1976-01-30

JPS5755695B2
(en)

1982-11-25

CA979842A
(en)

1975-12-16

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(en)

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Recovery of polyhydric alcohols and carboxylic acids salts from aqueous liquors

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(en)

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GB1371430A
(en)

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Process for preparing hydroxy citronellyl esters

GB1350611A
(en)

1974-04-18

Production of tetramethyl suberic acid

GB1344682A
(en)

1974-01-23

Process for producing dl/tryptophane

Legal Events

Date
Code
Title
Description

1974-11-27
PS
Patent sealed [section 19, patents act 1949]

1992-12-16
PE20
Patent expired after termination of 20 years

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