GB1046090A

GB1046090A – Method and apparatus for continuous grease manufacture
– Google Patents

GB1046090A – Method and apparatus for continuous grease manufacture
– Google Patents
Method and apparatus for continuous grease manufacture

Info

Publication number
GB1046090A

GB1046090A
GB51294/64A
GB5129464A
GB1046090A
GB 1046090 A
GB1046090 A
GB 1046090A
GB 51294/64 A
GB51294/64 A
GB 51294/64A
GB 5129464 A
GB5129464 A
GB 5129464A
GB 1046090 A
GB1046090 A
GB 1046090A
Authority
GB
United Kingdom
Prior art keywords
mixture
oil
lubricating oil
zone
tank
Prior art date
1963-12-24
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB51294/64A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Texaco Development Corp

Original Assignee
Texaco Development Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1963-12-24
Filing date
1964-12-16
Publication date
1966-10-19

1964-12-16
Application filed by Texaco Development Corp
filed
Critical
Texaco Development Corp

1966-10-19
Publication of GB1046090A
publication
Critical
patent/GB1046090A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M5/00—Solid or semi-solid compositions containing as the essential lubricating ingredient mineral lubricating oils or fatty oils and their use

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions

C10M2201/02—Water

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/02—Hydroxy compounds

C10M2207/021—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/022—Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms

C10M2207/122—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms monocarboxylic

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/121—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms

C10M2207/124—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of seven or less carbon atoms containing hydroxy groups; Ethers thereof

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids

C10M2207/128—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids containing hydroxy groups; Ethers thereof

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/10—Carboxylix acids; Neutral salts thereof

C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms

C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/28—Esters

C10M2207/282—Esters of (cyclo)aliphatic oolycarboxylic acids

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION

C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions

C10M2207/28—Esters

C10M2207/34—Esters having a hydrocarbon substituent of thirty or more carbon atoms, e.g. substituted succinic acid derivatives

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2010/00—Metal present as such or in compounds

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2010/00—Metal present as such or in compounds

C10N2010/02—Groups 1 or 11

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2010/00—Metal present as such or in compounds

C10N2010/04—Groups 2 or 12

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2010/00—Metal present as such or in compounds

C10N2010/06—Groups 3 or 13

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2010/00—Metal present as such or in compounds

C10N2010/08—Groups 4 or 14

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2050/00—Form in which the lubricant is applied to the material being lubricated

C10N2050/10—Semi-solids; greasy

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2070/00—Specific manufacturing methods for lubricant compositions

C—CHEMISTRY; METALLURGY

C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT

C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS

C10N2070/00—Specific manufacturing methods for lubricant compositions

C10N2070/02—Concentrating of additives

Abstract

In a continuous process for manufacturing lubricating grease including soap grease, saponifiable material and metal base are reacted in a reaction zone; the reaction product is dehydrated in a dehydration zone and the mixture is recycled from the bottom to the top of the dehydration zone through a shear valve so that the soap is simultaneously conditioned. Predetermined amounts of lubricating oil are added at each stage, but a lubricating oil hydrolysable under saponification conditions would not be added at this stage. The metal base may be the oxide, hydroxide or carbonate of an alkali metal, alkaline earth metal, magnesium, zinc, cobalt, manganese, aluminium or lead; the saponifiable material may be a fatty acid having 12 to 32 carbon atoms or an ester thereof, or a mixture thereof with a fatty acid having 1 to 6 carbon atoms; the lubricating oil may be a naphthenic and/or paraffinic mineral oil, a synthetic oil obtained by cracking a polymerization or a high molecular weight ether or ester, diesters such as di-2-ethylhexyl sebacate, or a mixture of any of the foregoing. As shown, saponifiable material, optionally containing lubricating oil, is introduced from tank 15, metal base in aqueous solution or oil slurry from tank 20, and lubricating oil mainly from tank 40 and, optionally, when more than one oil is to be used, tank 60. As shown, the lubricating oil may be introduced into the system at a number of points. The mixture is recycled through tubular reaction zone 1 by means of line 7 and pump 10 at a velocity giving highly turbulent flow, reaction taking place at 10-300 p.s.i.g. at 180 DEG F. or above. The reaction product is passed via line 26 and pump 27 to dehydration zone 30, maintained therein at above 225 DEG F. and recycled from bottom to top of the zone by pump 34 through shear valve 37 having a pressure drop of 10 to 200 p.s.i.g. across it. The volume of recycled grease mixture during the average residence time in the dehydration zone is at least five times the total average volume of mixture in the zone. Lubricating oil added at this stage comprises at least 25% of the mixture. The dehydrated grease mixture is withdrawn from line 33 via line 75, and oil added at this stage, comprising up to 90% of the total oil content, is advantageously used to cool the mixture. Also added at this stage are additives, from tank 90 and, in the case of cup greases, water of stabilization. The mixture is circulated through shear valve 81 and, if necessary, cooler 85. The product grease is taken off via line 87 and a further valve 88 after final required addition of oil have been made via line 71 and pump 72.

GB51294/64A
1963-12-24
1964-12-16
Method and apparatus for continuous grease manufacture

Expired

GB1046090A
(en)

Applications Claiming Priority (3)

Application Number
Priority Date
Filing Date
Title

US33316463A

1963-12-24
1963-12-24

BE678698

1966-03-30

US64643267A

1967-06-15
1967-06-15

Publications (1)

Publication Number
Publication Date

GB1046090A
true

GB1046090A
(en)

1966-10-19

Family
ID=27159154
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB51294/64A
Expired

GB1046090A
(en)

1963-12-24
1964-12-16
Method and apparatus for continuous grease manufacture

Country Status (5)

Country
Link

US
(1)

US3475335A
(en)

JP
(1)

JPS503767B1
(en)

BE
(1)

BE678698A
(en)

DE
(1)

DE1594633B1
(en)

GB
(1)

GB1046090A
(en)

Cited By (1)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US7829512B2
(en)

2003-10-17
2010-11-09
Exxonmobil Research And Engineering Company
Method and equipment for making a complex lithium grease

Families Citing this family (11)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4149981A
(en)

*

1977-01-12
1979-04-17
Kafarov Viktor V
Method of producing plastic and liquid lubricants

US4297227A
(en)

*

1979-03-02
1981-10-27
Texaco Inc.
Method for continuous grease manufacture

US4392967A
(en)

*

1981-08-11
1983-07-12
Exxon Research And Engineering Co.
Process for continuously manufacturing lubricating grease

US4444669A
(en)

*

1982-06-07
1984-04-24
Texaco Inc.
Method for continuous manufacture of high dropping point lithium complex soap grease

US5583284A
(en)

*

1994-09-13
1996-12-10
Mobil Oil Corporation
Method for monitoring grease consistency

GB9803367D0
(en)

1998-02-17
1998-04-15
Exxon Research Engineering Co
Lubricating grease composition and preparation

US9157045B2
(en)

*

2013-11-27
2015-10-13
Chevron U.S.A. Inc.
Continuous lithium complex grease manufacturing process with a borated additive

GR1009135B
(en)

*

2016-04-14
2017-10-12
Slider Α.Β.Ε.Ε. Παραγωγη Και Εμπορια Λιπαντικων
Method for automated grease production characterised by automatic pressure control at the saponification phase

US20190016984A1
(en)

2017-07-13
2019-01-17
Exxonmobil Research And Engineering Company
Continuous process for the manufacture of grease

US11661563B2
(en)

2020-02-11
2023-05-30
Nch Corporation
Composition and method of manufacturing and using extremely rheopectic sulfonate-based greases

CN115138277A
(en)

*

2022-06-27
2022-10-04
山东红星化工有限公司
Lubricating grease homogenizing and cooling method and device

Family Cites Families (15)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

NL142820C
(en)

*

1940-08-27

US2374913A
(en)

*

1941-08-15
1945-05-01
Standard Oil Dev Co
Preparation of lubricating greases and apparatus therefor

US2332202A
(en)

*

1941-08-19
1943-10-19
Standard Oil Dev Co
Lubricating grease manufacture and apparatus therefor

US2383906A
(en)

*

1942-10-28
1945-08-28
Standard Oil Dev Co
Improved manufacture

US2450220A
(en)

*

1945-05-03
1948-09-28
Texas Co
Texture-stable lithium base grease

BE505262A
(en)

*

1950-08-15

US2830022A
(en)

*

1953-06-30
1958-04-08
Texas Co
Method of grease manufacture with recycle cooling

US2886525A
(en)

*

1955-06-06
1959-05-12
Texas Co
Method of grease manufacture which comprises shearing the grease mixture at high temperatures

US2870090A
(en)

*

1956-06-25
1959-01-20
Texas Co
Method of grease manufacture comprising shearing

US3015624A
(en)

*

1958-12-22
1962-01-02
Texaco Inc
Method of preparing lithium soap greases

US3079341A
(en)

*

1958-12-22
1963-02-26
Texaco Inc
Rheopectic lithium soap grease and method of preparation therefor

US3068175A
(en)

*

1959-08-24
1962-12-11
Texaco Inc
Process for preparing complex calcium salt-calcium soap grease

US3068174A
(en)

*

1959-08-24
1962-12-11
Texaco Inc
Process for preparing complex calcium salt-calcium soap grease

US3117087A
(en)

*

1960-09-28
1964-01-07
Sinclair Research Inc
Method of making greases

US3242083A
(en)

*

1963-05-22
1966-03-22
Texaco Inc
Method of grease manufacture

1964

1964-12-16
GB
GB51294/64A
patent/GB1046090A/en
not_active
Expired

1964-12-23
DE
DE19641594633
patent/DE1594633B1/en
not_active
Withdrawn

1964-12-24
JP
JP39072632A
patent/JPS503767B1/ja
active
Pending

1966

1966-03-30
BE
BE678698D
patent/BE678698A/xx
unknown

1967

1967-06-15
US
US646432A
patent/US3475335A/en
not_active
Expired – Lifetime

Cited By (1)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US7829512B2
(en)

2003-10-17
2010-11-09
Exxonmobil Research And Engineering Company
Method and equipment for making a complex lithium grease

Also Published As

Publication number
Publication date

BE678698A
(en)

1966-09-01

JPS503767B1
(en)

1975-02-10

DE1594633B1
(en)

1971-11-04

US3475335A
(en)

1969-10-28

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