GB1091339A

GB1091339A – Method of separating components of low molecule weight from high-polymer compounds
– Google Patents

GB1091339A – Method of separating components of low molecule weight from high-polymer compounds
– Google Patents
Method of separating components of low molecule weight from high-polymer compounds

Info

Publication number
GB1091339A

GB1091339A
GB53829/65A
GB5382965A
GB1091339A
GB 1091339 A
GB1091339 A
GB 1091339A
GB 53829/65 A
GB53829/65 A
GB 53829/65A
GB 5382965 A
GB5382965 A
GB 5382965A
GB 1091339 A
GB1091339 A
GB 1091339A
Authority
GB
United Kingdom
Prior art keywords
steam
ejectors
vessel
maintained
vapours
Prior art date
1964-12-23
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB53829/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Vickers Zimmer AG

Original Assignee
Vickers Zimmer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1964-12-23
Filing date
1965-12-20
Publication date
1967-11-15

1965-12-20
Application filed by Vickers Zimmer AG
filed
Critical
Vickers Zimmer AG

1967-11-15
Publication of GB1091339A
publication
Critical
patent/GB1091339A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

B—PERFORMING OPERATIONS; TRANSPORTING

B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL

B01D—SEPARATION

B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping

B01D3/10—Vacuum distillation

B01D3/105—Vacuum distillation with the use of an ejector for creating the vacuum, the ejector being placed between evaporator or distillation devices

B—PERFORMING OPERATIONS; TRANSPORTING

B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL

B01D—SEPARATION

B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping

B01D3/10—Vacuum distillation

C—CHEMISTRY; METALLURGY

C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON

C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS

C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule

C08G63/78—Preparation processes

C08G63/785—Preparation processes characterised by the apparatus used

C—CHEMISTRY; METALLURGY

C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON

C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS

C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule

C08G69/46—Post-polymerisation treatment

Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC

Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y10S159/00—Concentrating evaporators

Y10S159/16—Vacuum

Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC

Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y10S203/00—Distillation: processes, separatory

Y10S203/16—Combination

Abstract

1,091,339. Separation of monomers and oligomers from high polymers. VICKERSZIMMER PLANUNG UND BAU VON INDUSTRIEANLAGEN A.G. Dec. 20, 1965 [Dec. 23, 1964], No. 53829/65. Heading B1B. Vaporisable components of low molecular weight are separated from high polymer compounds by vacuum distillation in a vessel 2 which is under the action of two steam jet ejectors 8 which are maintained at such a temperature as to prevent condensation occuring within the ejectors, the vapours formed together with the steam from the ejectors being condensed as an aqueous solution of the low molecular weight components in a water-cooled condenser 12. The jet ejectors are maintained at a temperature of 200C to 280C by either a steam-charged heating jacket which also surrounds pipe 7 or by feeding in superheated steam, the vapours being compressed to about 25 Torr by the ejectors whereby a pressure of about 2 Torr is maintained in the vessel 2. The propulsion seam is adjusted so that 15 weight units of steam are consumed per weight unit of extracted vapours. The polymerisation product requiring separation and entering through line 1, e.g. polymerised caprolactam or a polycondensate of ethylene glycol-terephthalate, is distributed over the surface of the vessel 2 as a thin film.

GB53829/65A
1964-12-23
1965-12-20
Method of separating components of low molecule weight from high-polymer compounds

Expired

GB1091339A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

DEZ0011247

1964-12-23

Publications (1)

Publication Number
Publication Date

GB1091339A
true

GB1091339A
(en)

1967-11-15

Family
ID=7621759
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB53829/65A
Expired

GB1091339A
(en)

1964-12-23
1965-12-20
Method of separating components of low molecule weight from high-polymer compounds

Country Status (7)

Country
Link

US
(1)

US3449220A
(en)

JP
(1)

JPS495830B1
(en)

CH
(1)

CH438218A
(en)

DE
(1)

DE1545221B2
(en)

FR
(1)

FR1461013A
(en)

GB
(1)

GB1091339A
(en)

NL
(2)

NL6516704A
(en)

Cited By (2)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

WO1996016711A1
(en)

*

1994-11-29
1996-06-06
Valery Grigorievich Tsegelsky
Facility for the vacuum distillation of a liquid product

RU2477394C1
(en)

*

2011-07-08
2013-03-10
Министерство образования и науки Российской Федерации Государственное образовательное учреждение высшего профессионального образования “Московский автомобильно-дорожный государственный технический университет (МАДИ)”
Multicomponent working liquid – simulator of borehole liquid for calibration bench

Families Citing this family (21)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US3642447A
(en)

*

1969-07-23
1972-02-15
Lynn Harold Hahn
Bromine purification process by addition of steam to the vapor phase

DE2135085C3
(en)

*

1971-07-14
1981-12-03
Basf Ag, 6700 Ludwigshafen

Process for the recovery of caprolactam from a mixture containing caprolactam and its oligomers

US3797551A
(en)

*

1971-07-21
1974-03-19
Agfa Gevaert Ag
Solidification of gelatin emulsions

USRE28937E
(en)

*

1971-11-18
1976-08-24
Allied Chemical Corporation
Control of viscosity and polycaproamide degradation during vacuum polycondensation

US4184924A
(en)

*

1974-08-19
1980-01-22
Ethyl Corporation
Apparatus for steam stripping polyvinyl chloride resins

DE2501348B2
(en)

*

1975-01-15
1981-04-09
Basf Ag, 6700 Ludwigshafen

Continuous process for the production of polyamides from epsilon-caprolactam

IT1100787B
(en)

*

1978-12-06
1985-09-28
Snia Viscosa

PROCESS AND EQUIPMENT FOR DEMONOMERIZATION OF POLYCAPROAMIDE

US4311642A
(en)

*

1980-09-17
1982-01-19
Allied Corporation
Recovery of caprolactam from nylon 6 oligomers

JPS63141692A
(en)

*

1986-12-03
1988-06-14
Konica Corp
Method and device for evaporation and concentration treatment of waste photographic processing liquid

AU603400B2
(en)

*

1986-12-17
1990-11-15
Konica Corporation
Method of treating photographic process waste liquor through concentration by evaporation and apparatus therefor

US5439560A
(en)

*

1990-02-22
1995-08-08
Konica Corporation
Low pressure evaporation concentrating apparatus for a photographic process waste disposl

DE4201046A1
(en)

*

1992-01-17
1993-07-22
Bayer Ag

METHOD FOR CLEANING POLYMER SOLUTIONS

US5531866A
(en)

*

1994-12-06
1996-07-02
Gas Research Institute
Water and organic constituent separator system and method

US6346173B2
(en)

*

1996-08-16
2002-02-12
Evgueni D. Petroukhine
Method for the vacuum distillation of a liquid product, particularly oil stock, (variants) and system for realizing the same

DE19844176C1
(en)

*

1998-09-25
2000-03-16
Ems Polyloy Gmbh

Process and device for vacuum demonomerization of polyamide 6 melts

ES2181663T3
(en)

2000-12-28
2003-03-01
Lundbeck & Co As H

PROCEDURE FOR THE PREPARATION OF PURE CITALOPRAM.

PL2297228T3
(en)

*

2008-06-20
2012-06-29
Basf Se
Continuous method for multi-staged drying and subsequent condensation of a polyamide granulate

US8540870B2
(en)

*

2009-06-25
2013-09-24
Uop Llc
Process for separating pitch from slurry hydrocracked vacuum gas oil

US8202480B2
(en)

*

2009-06-25
2012-06-19
Uop Llc
Apparatus for separating pitch from slurry hydrocracked vacuum gas oil

US9150470B2
(en)

2012-02-02
2015-10-06
Uop Llc
Process for contacting one or more contaminated hydrocarbons

CN104130401B
(en)

*

2013-05-01
2018-05-29
英威达纺织(英国)有限公司
Operation pressure control in nylon synthesis

Family Cites Families (8)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US2489703A
(en)

*

1947-04-24
1949-11-29
American Cyanamid Co
Evaporating aqueous solutions containing hcn

US2682499A
(en)

*

1950-03-20
1954-06-29
Kraft Foods Co
High vacuum distillation and drying system

US2793235A
(en)

*

1954-09-27
1957-05-21
Du Pont
Recovery of glycols from polyester production

DE1040018B
(en)

*

1956-05-17
1958-10-02
Basf Ag

Process for the recovery of dimethyl terephthalate

US2952675A
(en)

*

1958-07-01
1960-09-13
Inventa A G Fur Forschun Und P
Process of recovering epsilon-caprolactam from its polymer

US3017289A
(en)

*

1959-01-26
1962-01-16
Eastman Kodak Co
Method of preparing photographic materials

US3252502A
(en)

*

1962-01-19
1966-05-24
Allied Chem
Centrifugal wiped film evaporation process for viscous materials

US3258410A
(en)

*

1965-03-26
1966-06-28
Foster Grant Co Inc
Method of maintaining a monomer ratio in condensing polyamides

0

NL
NL135959D
patent/NL135959C/xx
active

1964

1964-12-23
DE
DE19641545221
patent/DE1545221B2/en
active
Pending

1965

1965-12-13
US
US513402A
patent/US3449220A/en
not_active
Expired – Lifetime

1965-12-14
FR
FR42219A
patent/FR1461013A/en
not_active
Expired

1965-12-20
GB
GB53829/65A
patent/GB1091339A/en
not_active
Expired

1965-12-22
NL
NL6516704A
patent/NL6516704A/xx
unknown

1965-12-22
CH
CH1769065A
patent/CH438218A/en
unknown

1965-12-23
JP
JP40079565A
patent/JPS495830B1/ja
active
Pending

Cited By (2)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

WO1996016711A1
(en)

*

1994-11-29
1996-06-06
Valery Grigorievich Tsegelsky
Facility for the vacuum distillation of a liquid product

RU2477394C1
(en)

*

2011-07-08
2013-03-10
Министерство образования и науки Российской Федерации Государственное образовательное учреждение высшего профессионального образования “Московский автомобильно-дорожный государственный технический университет (МАДИ)”
Multicomponent working liquid – simulator of borehole liquid for calibration bench

Also Published As

Publication number
Publication date

CH438218A
(en)

1967-06-30

DE1545221A1
(en)

1970-01-02

US3449220A
(en)

1969-06-10

NL6516704A
(en)

1966-06-24

DE1545221B2
(en)

1970-12-17

NL135959C
(en)

JPS495830B1
(en)

1974-02-09

FR1461013A
(en)

1966-12-02

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