GB1111807A

GB1111807A – Process for wet spinning elastic polyurethane fibers
– Google Patents

GB1111807A – Process for wet spinning elastic polyurethane fibers
– Google Patents
Process for wet spinning elastic polyurethane fibers

Info

Publication number
GB1111807A

GB1111807A
GB53912/65A
GB5391265A
GB1111807A
GB 1111807 A
GB1111807 A
GB 1111807A
GB 53912/65 A
GB53912/65 A
GB 53912/65A
GB 5391265 A
GB5391265 A
GB 5391265A
GB 1111807 A
GB1111807 A
GB 1111807A
Authority
GB
United Kingdom
Prior art keywords
filaments
bath
solution
coagulating bath
dimethylformamide
Prior art date
1964-12-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB53912/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Monsanto Co

Original Assignee
Monsanto Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1964-12-21
Filing date
1965-12-20
Publication date
1968-05-01

1965-12-20
Application filed by Monsanto Co
filed
Critical
Monsanto Co

1968-05-01
Publication of GB1111807A
publication
Critical
patent/GB1111807A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

D—TEXTILES; PAPER

D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING

D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS

D01D5/00—Formation of filaments, threads, or the like

D01D5/06—Wet spinning methods

D—TEXTILES; PAPER

D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING

D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS

D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof

D01F6/58—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products

D01F6/70—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from homopolycondensation products from polyurethanes

Abstract

1,111,807. Wet spinning elastomeric polyurethane filaments. MONSANTO CO. 20 Dec., 1965 [21 Dec., 1964], No. 83912/66. Heading B5B. Elastomeric polyurethane filaments are produced by wet spinning a solution of a segmented polyurethane polymer in an organic solvent into a coagulating bath consisting of water and the organic solvent, drawing the filaments upwards along a vertical path from the spinneret face through the coagulating bath a distance of 0À5 to 3À0, preferably 1À5 to 2À0 inches at a rate of withdrawal which will result in the filaments remaining in the bath for 0À025 to 0À2 second, preferably 0À075 to 0À1 second, so that the filaments emerge from the bath in a direction which is normal to the surface of the coagulating bath and forwarding the filaments for further processing after their emergence from the coagulating bath. The solvent may be dimethylformamide or dimethylacetamide, dimethylsulphoxide or hexamethphosphoramide. The aqueous coagulating bath is preferably maintained at about 60 to 90 C. and the percentage of organic solvent in the bath may be about 1 to 40%. In an example, the polymer solution is formed by first forming a solution of a ” prepolymer ” by reacting a polycaprolactone with 4,41 methylenediphenyl diisocyanate in dimethylformamide solvent and the solution is added to a solution of ethylene diamine in dimethylformamide to give a spinning dope containing 15% solids. In all the examples the filaments formed are washed, dried and taken up after their emergence from the bath.

GB53912/65A
1964-12-21
1965-12-20
Process for wet spinning elastic polyurethane fibers

Expired

GB1111807A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US419779A

US3388200A
(en)

1964-12-21
1964-12-21
Process for wet spinning elastic fibers

Publications (1)

Publication Number
Publication Date

GB1111807A
true

GB1111807A
(en)

1968-05-01

Family
ID=23663726
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB53912/65A
Expired

GB1111807A
(en)

1964-12-21
1965-12-20
Process for wet spinning elastic polyurethane fibers

Country Status (9)

Country
Link

US
(1)

US3388200A
(en)

BE
(1)

BE674131A
(en)

CH
(1)

CH480455A
(en)

DE
(1)

DE1660468A1
(en)

FR
(1)

FR1461054A
(en)

GB
(1)

GB1111807A
(en)

IL
(1)

IL24836A
(en)

LU
(1)

LU50116A1
(en)

NL
(1)

NL6516600A
(en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US3548047A
(en)

*

1967-02-23
1970-12-15
Union Carbide Corp
Lubrication of spandex yarns

US5183614A
(en)

*

1989-01-26
1993-02-02
E. I. Du Pont De Nemours And Company
Method for producing x-ray detectable spandex fibers

DE102006059932A1
(en)

*

2006-12-19
2008-06-26
Robert Bosch Gmbh

Method and device for producing a strand-shaped extrudate

Family Cites Families (2)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

NL245712A
(en)

*

1958-11-24
1900-01-01

US3036878A
(en)

*

1959-09-25
1962-05-29
Globe Mfg Company
Polyurethanes

1964

1964-12-21
US
US419779A
patent/US3388200A/en
not_active
Expired – Lifetime

1965

1965-12-20
GB
GB53912/65A
patent/GB1111807A/en
not_active
Expired

1965-12-20
NL
NL6516600A
patent/NL6516600A/xx
unknown

1965-12-20
IL
IL24836A
patent/IL24836A/en
unknown

1965-12-21
BE
BE674131D
patent/BE674131A/xx
unknown

1965-12-21
DE
DE19651660468
patent/DE1660468A1/en
active
Pending

1965-12-21
LU
LU50116A
patent/LU50116A1/xx
unknown

1965-12-21
FR
FR43122A
patent/FR1461054A/en
not_active
Expired

1965-12-21
CH
CH1757065A
patent/CH480455A/en
not_active
IP Right Cessation

Also Published As

Publication number
Publication date

LU50116A1
(en)

1966-06-21

DE1660468A1
(en)

1971-01-14

IL24836A
(en)

1969-07-30

NL6516600A
(en)

1966-06-22

US3388200A
(en)

1968-06-11

FR1461054A
(en)

1966-12-10

CH480455A
(en)

1969-10-31

BE674131A
(en)

1966-06-21

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(en)

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Process for producing melt-spun elastomeric filaments

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