GB1197271A

GB1197271A – Process for the Purification of Finely Divided Oxides
– Google Patents

GB1197271A – Process for the Purification of Finely Divided Oxides
– Google Patents
Process for the Purification of Finely Divided Oxides

Info

Publication number
GB1197271A

GB1197271A
GB2766/68A
GB276668A
GB1197271A
GB 1197271 A
GB1197271 A
GB 1197271A
GB 2766/68 A
GB2766/68 A
GB 2766/68A
GB 276668 A
GB276668 A
GB 276668A
GB 1197271 A
GB1197271 A
GB 1197271A
Authority
GB
United Kingdom
Prior art keywords
oxide
oxides
steam
purification
finely divided
Prior art date
1967-01-21
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB2766/68A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Evonik Operations GmbH

Original Assignee
Degussa GmbH
Deutsche Gold und Silber Scheideanstalt
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1967-01-21
Filing date
1968-01-18
Publication date
1970-07-01

1968-01-18
Application filed by Degussa GmbH, Deutsche Gold und Silber Scheideanstalt
filed
Critical
Degussa GmbH

1970-07-01
Publication of GB1197271A
publication
Critical
patent/GB1197271A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR

C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS

C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties

C09C3/006—Combinations of treatments provided for in groups C09C3/04 – C09C3/12

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B13/00—Oxygen; Ozone; Oxides or hydroxides in general

C01B13/14—Methods for preparing oxides or hydroxides in general

C01B13/145—After-treatment of oxides or hydroxides, e.g. pulverising, drying, decreasing the acidity

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B33/00—Silicon; Compounds thereof

C01B33/113—Silicon oxides; Hydrates thereof

C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid

C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof

C01B33/181—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process

C01B33/183—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by a dry process by oxidation or hydrolysis in the vapour phase of silicon compounds such as halides, trichlorosilane, monosilane

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F

C01G23/00—Compounds of titanium

C01G23/04—Oxides; Hydroxides

C01G23/047—Titanium dioxide

C01G23/07—Producing by vapour phase processes, e.g. halide oxidation

C01G23/075—Evacuation and cooling of the gaseous suspension containing the oxide; Desacidification and elimination of gases occluded in the separated oxide

C—CHEMISTRY; METALLURGY

C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR

C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS

C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties

C09C3/04—Physical treatment, e.g. grinding, treatment with ultrasonic vibrations

C09C3/043—Drying, calcination

C—CHEMISTRY; METALLURGY

C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR

C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS

C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties

C09C3/06—Treatment with inorganic compounds

C—CHEMISTRY; METALLURGY

C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR

C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS

C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties

C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

C01P2006/00—Physical properties of inorganic compounds

C01P2006/12—Surface area

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

C01P2006/00—Physical properties of inorganic compounds

C01P2006/80—Compositional purity

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS

C01P2006/00—Physical properties of inorganic compounds

C01P2006/90—Other properties not specified above

Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE

Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

Y02P20/00—Technologies relating to chemical industry

Y02P20/10—Process efficiency

Y02P20/129—Energy recovery, e.g. by cogeneration, H2recovery or pressure recovery turbines

Abstract

1,197,271. Purification of oxides. DEUTSCHE GOLD – UND SILBER – SCHEIDEANSTALT. 18 Jan., 1968 [21 Jan., 1967], No. 2766/68. Headings C1A and C1N. Finely divided oxides or mixtures of oxides produced by vapour phase oxidation or hydrolysis of chlorides, are purified by introducing the oxide into a treatment zone heated to 400-600‹ C. in which it descends under gravity in countercurrent to an ascending stream of a mixture of steam and an inert gas, the flow of gas being insufficient to fluidize the oxide. The gas mixture is preferably of steam and compressed air preheated to 120‹ C. The oxide may be SiO 2 of s.a. 200 m2/gm., TiO 2 , or Al 2 O 3 of s.a. 80 m2/gm. The treatment zone may be a vertical tube widened at its upper and lower ends. It may be heated externally by electric heating coils or internally by H 2 burners, the flames being screened from the solid (in this case, steam for the treatment is produced by the burners). The pH of a 4% aqueous dispersion of the oxide is increased from 1À9 to 4 or 4À2 (for SiO 2 ) or from 1À5 to 8À2 (for Al 2 O 3 ).

GB2766/68A
1967-01-21
1968-01-18
Process for the Purification of Finely Divided Oxides

Expired

GB1197271A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

DED0052080

1967-01-21

Publications (1)

Publication Number
Publication Date

GB1197271A
true

GB1197271A
(en)

1970-07-01

Family
ID=7053890
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB2766/68A
Expired

GB1197271A
(en)

1967-01-21
1968-01-18
Process for the Purification of Finely Divided Oxides

Country Status (6)

Country
Link

JP
(1)

JPS4813832B1
(en)

BE
(1)

BE709670A
(en)

DE
(1)

DE1642994A1
(en)

FR
(1)

FR1554066A
(en)

GB
(1)

GB1197271A
(en)

NL
(1)

NL6800730A
(en)

Cited By (18)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

EP0123669A2
(en)

*

1983-03-24
1984-10-31
VOEST-ALPINE Aktiengesellschaft
Method of separating borates from magnesium hydroxide obtained from sea water, and apparatus for carrying out the method

EP0129015A2
(en)

*

1983-06-10
1984-12-27
Degussa Aktiengesellschaft
Pyrogenically produced silicon dioxide, process for its preparation and use

EP0709340A1
(en)

*

1994-10-27
1996-05-01
Shin-Etsu Chemical Co., Ltd.
Method for purifying fine particulate silica

US5707599A
(en)

*

1996-02-13
1998-01-13
Santiam Electroactive Materials
Process for purifying tantalum oxide and other metal oxides

US5855860A
(en)

*

1994-10-27
1999-01-05
Shin-Etsu Chemical Co., Ltd.
Method for porifying fine particulate silica

WO2005019107A1
(en)

*

2003-08-20
2005-03-03
Degussa Ag
Purification of finely divided, pyrogenically prepared metal oxide particles

CN100447083C
(en)

*

2003-08-20
2008-12-31
德古萨股份公司
Purification of finely divided, pyrogenically prepared metal oxide particles

WO2017103170A1
(en)

*

2015-12-18
2017-06-22
Heraeus Quarzglas Gmbh & Co. Kg
Steam treatment of silica powder during the production of silica glass

US10618833B2
(en)

2015-12-18
2020-04-14
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a synthetic quartz glass grain

US10676388B2
(en)

2015-12-18
2020-06-09
Heraeus Quarzglas Gmbh & Co. Kg
Glass fibers and pre-forms made of homogeneous quartz glass

US10730780B2
(en)

2015-12-18
2020-08-04
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a quartz glass body in a multi-chamber oven

WO2021121557A1
(en)

2019-12-17
2021-06-24
Wacker Chemie Ag
Fluidized-bed reactor for the control of the dwell time distribution in continuously operated fluidized beds

US11053152B2
(en)

2015-12-18
2021-07-06
Heraeus Quarzglas Gmbh & Co. Kg
Spray granulation of silicon dioxide in the preparation of quartz glass

US11236002B2
(en)

2015-12-18
2022-02-01
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of an opaque quartz glass body

US11299417B2
(en)

2015-12-18
2022-04-12
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a quartz glass body in a melting crucible of refractory metal

US11339076B2
(en)

2015-12-18
2022-05-24
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of carbon-doped silicon dioxide granulate as an intermediate in the preparation of quartz glass

US11492282B2
(en)

2015-12-18
2022-11-08
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of quartz glass bodies with dew point monitoring in the melting oven

US11492285B2
(en)

2015-12-18
2022-11-08
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of quartz glass bodies from silicon dioxide granulate

Families Citing this family (3)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

RU2136596C1
(en)

1993-11-25
1999-09-10
Сумитомо Кемикал Компани, Лимитед
Method of preparing alpha-aluminum powder and alpha-aluminum powder

JP5553601B2
(en)

*

2007-07-27
2014-07-16
東邦チタニウム株式会社

Method for producing titanium oxide powder

CN109205629B
(en)

*

2018-11-21
2023-11-14
浙江富士特硅材料有限公司
Circulation formula gas phase method white carbon black deacidification system

1967

1967-01-21
DE
DE19671642994
patent/DE1642994A1/en
active
Pending

1968

1968-01-17
NL
NL6800730A
patent/NL6800730A/xx
unknown

1968-01-18
GB
GB2766/68A
patent/GB1197271A/en
not_active
Expired

1968-01-18
FR
FR1554066D
patent/FR1554066A/fr
not_active
Expired

1968-01-19
BE
BE709670D
patent/BE709670A/xx
not_active
IP Right Cessation

1968-01-22
JP
JP43003674A
patent/JPS4813832B1/ja
active
Pending

Cited By (22)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

EP0123669A2
(en)

*

1983-03-24
1984-10-31
VOEST-ALPINE Aktiengesellschaft
Method of separating borates from magnesium hydroxide obtained from sea water, and apparatus for carrying out the method

EP0123669A3
(en)

*

1983-03-24
1987-12-02
VOEST-ALPINE Aktiengesellschaft
Method of separating borates from magnesium hydroxide obtained from sea water, and apparatus for carrying out the method

EP0129015A2
(en)

*

1983-06-10
1984-12-27
Degussa Aktiengesellschaft
Pyrogenically produced silicon dioxide, process for its preparation and use

EP0129015A3
(en)

*

1983-06-10
1988-09-07
Degussa Aktiengesellschaft
Pyrogenically produced silicon dioxide, process for its preparation and use

EP0709340A1
(en)

*

1994-10-27
1996-05-01
Shin-Etsu Chemical Co., Ltd.
Method for purifying fine particulate silica

US5855860A
(en)

*

1994-10-27
1999-01-05
Shin-Etsu Chemical Co., Ltd.
Method for porifying fine particulate silica

US5707599A
(en)

*

1996-02-13
1998-01-13
Santiam Electroactive Materials
Process for purifying tantalum oxide and other metal oxides

WO2005019107A1
(en)

*

2003-08-20
2005-03-03
Degussa Ag
Purification of finely divided, pyrogenically prepared metal oxide particles

CN100447083C
(en)

*

2003-08-20
2008-12-31
德古萨股份公司
Purification of finely divided, pyrogenically prepared metal oxide particles

US7785560B2
(en)

2003-08-20
2010-08-31
Evonik Degussa Gmbh
Purification of finely divided, pyrogenically prepared metal oxide particles

WO2017103170A1
(en)

*

2015-12-18
2017-06-22
Heraeus Quarzglas Gmbh & Co. Kg
Steam treatment of silica powder during the production of silica glass

US10618833B2
(en)

2015-12-18
2020-04-14
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a synthetic quartz glass grain

US10676388B2
(en)

2015-12-18
2020-06-09
Heraeus Quarzglas Gmbh & Co. Kg
Glass fibers and pre-forms made of homogeneous quartz glass

US10730780B2
(en)

2015-12-18
2020-08-04
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a quartz glass body in a multi-chamber oven

US11053152B2
(en)

2015-12-18
2021-07-06
Heraeus Quarzglas Gmbh & Co. Kg
Spray granulation of silicon dioxide in the preparation of quartz glass

US11236002B2
(en)

2015-12-18
2022-02-01
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of an opaque quartz glass body

US11299417B2
(en)

2015-12-18
2022-04-12
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a quartz glass body in a melting crucible of refractory metal

US11339076B2
(en)

2015-12-18
2022-05-24
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of carbon-doped silicon dioxide granulate as an intermediate in the preparation of quartz glass

US11492282B2
(en)

2015-12-18
2022-11-08
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of quartz glass bodies with dew point monitoring in the melting oven

US11492285B2
(en)

2015-12-18
2022-11-08
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of quartz glass bodies from silicon dioxide granulate

US11708290B2
(en)

2015-12-18
2023-07-25
Heraeus Quarzglas Gmbh & Co. Kg
Preparation of a quartz glass body in a multi-chamber oven

WO2021121557A1
(en)

2019-12-17
2021-06-24
Wacker Chemie Ag
Fluidized-bed reactor for the control of the dwell time distribution in continuously operated fluidized beds

Also Published As

Publication number
Publication date

NL6800730A
(en)

1968-07-22

FR1554066A
(en)

1968-12-09

DE1642994A1
(en)

1971-06-03

BE709670A
(en)

1968-05-30

JPS4813832B1
(en)

1973-05-01

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Legal Events

Date
Code
Title
Description

1970-11-11
PS
Patent sealed

1988-02-24
PE20
Patent expired after termination of 20 years

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