GB1459909A – Device for automatic analysis by mass spectrometry
– Google Patents
GB1459909A – Device for automatic analysis by mass spectrometry
– Google Patents
Device for automatic analysis by mass spectrometry
Info
Publication number
GB1459909A
GB1459909A
GB4048474A
GB4048474A
GB1459909A
GB 1459909 A
GB1459909 A
GB 1459909A
GB 4048474 A
GB4048474 A
GB 4048474A
GB 4048474 A
GB4048474 A
GB 4048474A
GB 1459909 A
GB1459909 A
GB 1459909A
Authority
GB
United Kingdom
Prior art keywords
valve
pipe
pipes
cell
traced
Prior art date
1973-09-25
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4048474A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
RECH ET DACTIVITES PETROLIERES
Original Assignee
RECH ET DACTIVITES PETROLIERES
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1973-09-25
Filing date
1974-09-17
Publication date
1976-12-31
1974-09-17
Application filed by RECH ET DACTIVITES PETROLIERES
filed
Critical
RECH ET DACTIVITES PETROLIERES
1976-12-31
Publication of GB1459909A
publication
Critical
patent/GB1459909A/en
Status
Expired
legal-status
Critical
Current
Links
Espacenet
Global Dossier
Discuss
Classifications
G—PHYSICS
G01—MEASURING; TESTING
G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N1/00—Sampling; Preparing specimens for investigation
G01N1/02—Devices for withdrawing samples
G01N1/10—Devices for withdrawing samples in the liquid or fluent state
G01N1/20—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials
G01N1/2035—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping
H—ELECTRICITY
H01—ELECTRIC ELEMENTS
H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
H01J49/00—Particle spectrometers or separator tubes
H01J49/02—Details
H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components
G—PHYSICS
G01—MEASURING; TESTING
G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G01N1/00—Sampling; Preparing specimens for investigation
G01N1/02—Devices for withdrawing samples
G01N1/10—Devices for withdrawing samples in the liquid or fluent state
G01N2001/1031—Sampling from special places
G01N2001/1037—Sampling from special places from an enclosure (hazardous waste, radioactive)
Abstract
1459909 Automatic analysis of flowing twophase mixtures ENTREPRISE DE RECHERCHES ET D’ACTIVITES PETROLIERES ELF 17 Sept 1974 [25 Sept 1973] 40484/74 Heading G1B A device for automatic analysis by mass spectrometry of two-phase mixtures which flow continuously through main pipes 2, 4 in for example a cracking plant comprises pipes 18, 22 &c. constituting a plurality of primary loops Bi (B 1 , B 2 shown), each of the primary loops being connected to a different one of the main pipes and to a recycling circuit in the direction of 27, each loop being fitted with a flow regulating valve 6, 10 and a flowmeter 8, 12 in series, the primary loops being traced, pipes Ti each connecting a branch point in a primary loop Bi to a pneumatic valve Vj (30 as shown) through a dust filter 26, 28 and a needle valve 32, 34 for regulating the flow-rate, the pneumatic valve(s) each for operably connecting one of the pipes Ti to one end of a further traced pipe T’, a sampling cell 40 at the other end of pipe T’, a sampling pipe T” for connecting one outlet of the cell 40 to the recycle circuit through a delivery valve V’ and a flowmeter 42 in series, means 46 for measuring the pressure in the cell 40, means for regulating the pressure in the cell by regulating the opening of valve V’ in response to a difference in pressure between the pressure measured by 46 and a reference pressure, a further traced pipe for connecting cell 40 to a further pneumatic valve V”, a traced capillary tube T”‘ for connecting valve V” to a chamber E, pumping means 58, 60 for creating a vacuum within chamber E, a pipe for connecting chamber E to the ionization chamber 62 of a mass spectrometer, electronic means (not shown) for simultaneously initiating the application of voltage to the acceleration electrodes of the mass spectrometer and the opening of the pneumatic valve V”, and means for initiating the selective opening of the valves Vj. The pipe “tracing” may comprise electrical resistance heating wire or a steam-fed copper pipe wound around the pipe to be traced, or a steam-fed sleeve concentric with the pipe. Fig. 3 (not shown) relates to the arrangement of eight pneumatic valves connectable in series, each valve having an inlet connected to one of a series of eight pipes carrying mixture to be analyzed, the valves being selectively operated by respective pairs of electrovalves, each pair of electrovalves being operable to connect one of the two inputs of the valve to the valve output.
GB4048474A
1973-09-25
1974-09-17
Device for automatic analysis by mass spectrometry
Expired
GB1459909A
(en)
Applications Claiming Priority (1)
Application Number
Priority Date
Filing Date
Title
FR7334263A
FR2245249A5
(en)
1973-09-25
1973-09-25
Publications (1)
Publication Number
Publication Date
GB1459909A
true
GB1459909A
(en)
1976-12-31
Family
ID=9125513
Family Applications (1)
Application Number
Title
Priority Date
Filing Date
GB4048474A
Expired
GB1459909A
(en)
1973-09-25
1974-09-17
Device for automatic analysis by mass spectrometry
Country Status (9)
Country
Link
US
(1)
US3943363A
(en)
JP
(1)
JPS5740975B2
(en)
BE
(1)
BE819367A
(en)
CA
(1)
CA1023472A
(en)
DE
(1)
DE2445124C3
(en)
FR
(1)
FR2245249A5
(en)
GB
(1)
GB1459909A
(en)
IT
(1)
IT1022244B
(en)
NL
(1)
NL7411676A
(en)
Families Citing this family (17)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US4207465A
(en)
*
1978-07-03
1980-06-10
Phillips Petroleum Company
Isotope analysis with a mass spectrometer using small samples
US4380701A
(en)
*
1980-10-02
1983-04-19
Texaco Inc.
Nuclear well logging with neutron source and separate spaced radiation detectors to determine silicon/oxygen ratio
US4960992A
(en)
*
1983-08-30
1990-10-02
Research Corporation Technologies
Method and means for vaporizing liquids by means of heating a sample capillary tube for detection or analysis
US4814612A
(en)
*
1983-08-30
1989-03-21
Research Corporation
Method and means for vaporizing liquids for detection or analysis
US4861989A
(en)
*
1983-08-30
1989-08-29
Research Corporation Technologies, Inc.
Ion vapor source for mass spectrometry of liquids
US4722830A
(en)
*
1986-05-05
1988-02-02
General Electric Company
Automated multiple stream analysis system
US4791291A
(en)
*
1986-07-14
1988-12-13
The Dow Chemical Company
Mass spectrometer sampling system for a liquid stream
FR2645966B1
(en)
*
1989-04-18
1991-06-07
Commissariat Energie Atomique
INSTALLATION OF CONTINUOUS AND REAL-TIME MEASUREMENTS, METAL MASSES IN ACID SOLUTION, AND THE ACIDITY OF THIS SOLUTION
JP2892795B2
(en)
*
1989-09-12
1999-05-17
エーザイ株式会社
Mobile phase conversion method and apparatus in high performance liquid chromatography mass spectrometry
JPH03282252A
(en)
*
1990-03-30
1991-12-12
Hitachi Ltd
Apparatus for analyzing very minute amount of element of plasma
DE4133300C2
(en)
*
1991-10-08
1996-07-11
Fraunhofer Ges Forschung
Method and device for determining strippable substances from liquids
US5237175A
(en)
*
1992-02-26
1993-08-17
Varian Associates, Inc.
Reagent gas control for an ion trap mass spectrometer used in the chemical ionization mode
US5376335A
(en)
*
1993-04-30
1994-12-27
Gleaves; John T.
Apparatus for study and analysis of products of catalytic reaction
US6063633A
(en)
*
1996-02-28
2000-05-16
The University Of Houston
Catalyst testing process and apparatus
CN109536755B
(en)
*
2018-12-13
2020-11-27
中国兵器工业第五九研究所
Intelligent control system for air content of aluminum alloy melt
CN112657960B
(en)
*
2020-12-16
2022-11-22
华能海南发电股份有限公司电力检修分公司
One set of system of sweeping to denitration export net sampling device
CN114152475B
(en)
*
2022-02-07
2022-04-08
东营石油技术与装备产业研究院有限公司
Closed type high-efficiency sampling device for petroleum detection
Family Cites Families (2)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
US2977471A
(en)
*
1958-09-25
1961-03-28
Socony Mobil Oil Co Inc
Apparatus for automatically operating a mass spectrometer
GB979958A
(en)
*
1963-06-05
1965-01-06
Exxon Research Engineering Co
Automatic computer for use with mass spectrometers
1973
1973-09-25
FR
FR7334263A
patent/FR2245249A5/fr
not_active
Expired
1974
1974-08-29
BE
BE148056A
patent/BE819367A/en
not_active
IP Right Cessation
1974-09-03
NL
NL7411676A
patent/NL7411676A/en
active
Search and Examination
1974-09-17
US
US05/506,730
patent/US3943363A/en
not_active
Expired – Lifetime
1974-09-17
GB
GB4048474A
patent/GB1459909A/en
not_active
Expired
1974-09-20
DE
DE2445124A
patent/DE2445124C3/en
not_active
Expired
1974-09-23
CA
CA209,963A
patent/CA1023472A/en
not_active
Expired
1974-09-24
IT
IT27622/74A
patent/IT1022244B/en
active
1974-09-25
JP
JP49110403A
patent/JPS5740975B2/ja
not_active
Expired
Also Published As
Publication number
Publication date
NL7411676A
(en)
1975-03-27
DE2445124B2
(en)
1978-07-20
DE2445124C3
(en)
1979-03-29
US3943363A
(en)
1976-03-09
DE2445124A1
(en)
1975-04-10
JPS5740975B2
(en)
1982-08-31
IT1022244B
(en)
1978-03-20
JPS5061286A
(en)
1975-05-26
FR2245249A5
(en)
1975-04-18
BE819367A
(en)
1974-12-16
CA1023472A
(en)
1977-12-27
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Legal Events
Date
Code
Title
Description
1977-09-21
PS
Patent sealed [section 19, patents act 1949]
1989-05-10
PCNP
Patent ceased through non-payment of renewal fee