GB1517673A – Process for the production of thermoformable polyisocyanurate foams
– Google Patents
GB1517673A – Process for the production of thermoformable polyisocyanurate foams
– Google Patents
Process for the production of thermoformable polyisocyanurate foams
Info
Publication number
GB1517673A
GB1517673A
GB7340/77A
GB734077A
GB1517673A
GB 1517673 A
GB1517673 A
GB 1517673A
GB 7340/77 A
GB7340/77 A
GB 7340/77A
GB 734077 A
GB734077 A
GB 734077A
GB 1517673 A
GB1517673 A
GB 1517673A
Authority
GB
United Kingdom
Prior art keywords
polyether
foam
component
carried out
polyisocyanate
Prior art date
1976-02-24
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB7340/77A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1976-02-24
Filing date
1977-02-22
Publication date
1978-07-12
1977-02-22
Application filed by Bayer AG
filed
Critical
Bayer AG
1978-07-12
Publication of GB1517673A
publication
Critical
patent/GB1517673A/en
Status
Expired
legal-status
Critical
Current
Links
Espacenet
Global Dossier
Discuss
Classifications
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G18/00—Polymeric products of isocyanates or isothiocyanates
C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
C08G18/72—Polyisocyanates or polyisothiocyanates
C08G18/80—Masked polyisocyanates
C08G18/8003—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen
C08G18/8006—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32
C08G18/8009—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203
C08G18/8012—Masked polyisocyanates masked with compounds having at least two groups containing active hydrogen with compounds of C08G18/32 with compounds of C08G18/3203 with diols
C08G18/8019—Masked aromatic polyisocyanates
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G18/00—Polymeric products of isocyanates or isothiocyanates
C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
C08G18/40—High-molecular-weight compounds
C08G18/48—Polyethers
C08G18/4833—Polyethers containing oxyethylene units
C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G18/00—Polymeric products of isocyanates or isothiocyanates
C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
C08G18/6666—Compounds of group C08G18/48 or C08G18/52
C08G18/667—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38
C08G18/6674—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of group C08G18/3203
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G18/00—Polymeric products of isocyanates or isothiocyanates
C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
C08G18/72—Polyisocyanates or polyisothiocyanates
C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G18/00—Polymeric products of isocyanates or isothiocyanates
C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
C08G18/72—Polyisocyanates or polyisothiocyanates
C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
C08G18/78—Nitrogen
C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
C08G18/797—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing carbodiimide and/or uretone-imine groups
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G2110/00—Foam properties
C08G2110/0025—Foam properties rigid
C—CHEMISTRY; METALLURGY
C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
C08G2110/00—Foam properties
C08G2110/0041—Foam properties having specified density
C08G2110/005—< 50kg/m3 C—CHEMISTRY; METALLURGY C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS C08G2110/00—Foam properties C08G2110/0041—Foam properties having specified density C08G2110/0058—≥50 and <150kg>-diisocyanatodiphenylmethane. In polyether component (a) preferably at least 10% wt. of the OH groups are primary OH groups. Part of the polyether component (a) may be replaced by compounds ofM.Wt. 800 to 10,000 containing NCO-reactive hydrogen atoms, e.g. polyesters, polyamines, polythiols, polycarboxylic acids, polyacetals, polycarbonates and OH-containing polybutadienes. The dihydric alcohol (b) may be a C2-C8 alkane diol, 1,4-bis-hydroxymethylcyclohexane, di-, tri-, tetra- or poly-ethylene, – propylene or -butylene glycols. The blowing agent may be water and/or a volatile inert organic substance. Suitable trimerization catalysts include quaternary ammonium hydroxides, alkali metal hydroxides, alkali metal alkoxides, alkali metal salts of carboxylic acids, lead octoate and certain tertiary amines, e.g. N-(2- dimethyl-aminoethyl)-N<1>-methyl piperazine and tris – (3 – dimethylaminopropyl) – hexahydrotriazine. The above catalysts may be used together with conventional urethane catalysts. Conventional additives such as foam stabilizers, cell regulators and stabilizers may be added. The process is preferably carried out by the oneshot procedure and it may be carried out continuously or discontinuously. The cell diameter of the foam is generally from 0À3 to 2À5 mm. Thermoforming of the foam may be carried out by bending, pressing or stamping and the heating may be carried out in hot air ovens, microwave or infra-red heating channels or contact hot plates. The thermoforming temperature is generally from 150 to 210 C. The thermoforming may be carried out continuously or discontinuously and the foam may be profiled. In a typical example a rigid polyisocyanurate foam is prepared by vigorously mixing a component (A) comprising an ethylene oxide/propylene oxide/trimethylolpropane polyether of OH number 56, ethane-1,2-diol, water, tris – (dimethylaminopropyl) -hexahydrotriazine, potassium acetate, permethylated diethylenetriamine, a polyether polysiloxane stabilizer and a phenylmethyl polysiloxane cell regulator, with a component (B) comprising monofluorotrichloromethane and diisocyanatodiphenylmethane consisting of 90% wt. of 4,4<1>-isomers and 10% wt. of 2,41-isomers modified with 14% wt. of tripropylene glycol.
GB7340/77A
1976-02-24
1977-02-22
Process for the production of thermoformable polyisocyanurate foams
Expired
GB1517673A
(en)
Applications Claiming Priority (1)
Application Number
Priority Date
Filing Date
Title
DE2607380A
DE2607380C3
(en)
1976-02-24
1976-02-24
Process for the production of thermoformable polyisocyanurate foams
Publications (1)
Publication Number
Publication Date
GB1517673A
true
GB1517673A
(en)
1978-07-12
Family
ID=5970687
Family Applications (1)
Application Number
Title
Priority Date
Filing Date
GB7340/77A
Expired
GB1517673A
(en)
1976-02-24
1977-02-22
Process for the production of thermoformable polyisocyanurate foams
Country Status (10)
Country
Link
US
(1)
US4129697A
(en)
JP
(1)
JPS52103495A
(en)
BE
(1)
BE851698A
(en)
BR
(1)
BR7700994A
(en)
DE
(1)
DE2607380C3
(en)
ES
(1)
ES456177A1
(en)
GB
(1)
GB1517673A
(en)
IT
(1)
IT1083472B
(en)
NL
(1)
NL7701943A
(en)
SE
(1)
SE434161B
(en)
Cited By (1)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
GB2249793A
(en)
*
1990-11-16
1992-05-20
Basf Corp
Integral-skin rigid urethane foam
Families Citing this family (52)
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Publication number
Priority date
Publication date
Assignee
Title
US4169921A
(en)
*
1973-01-11
1979-10-02
The Celotex Corporation
Polyisocyanurate
US4125505A
(en)
*
1976-07-06
1978-11-14
Union Carbide Corporation
Polymer/polyols from high ethylene oxide content polyols
DE2722400C2
(en)
*
1977-05-17
1985-05-30
Bayer Ag, 5090 Leverkusen
Process for the production of heat-resistant, bubble-free plastics containing isocyanurate groups
US4311801A
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*
1978-06-01
1982-01-19
The Celotex Corporation
Polyisocyanurate foam and process therefor
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1978-06-01
1980-07-15
The Celotex Corporation
Polyisocyanurate foam laminate
JPS5552313A
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1978-10-09
1980-04-16
Takeda Chem Ind Ltd
Manufacture of urethane-modified rigid isocyanurate foam
JPS5565214A
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*
1978-11-10
1980-05-16
Bridgestone Corp
Preparation of flame-resistant polyisocyanurate foam
DE2856456A1
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*
1978-12-28
1980-07-17
Basf Ag
METHOD FOR PRODUCING POLYURETHANE HARD FOAM MATERIALS
DE2915474C2
(en)
*
1979-04-17
1986-05-15
Hans-Georg Ring
Rigid composite laminate, process for its production and use as a finished headliner for automobiles
US4272618A
(en)
*
1979-04-30
1981-06-09
Texaco Development Corp.
Heat stable reaction injection molded elastomers
US4299924A
(en)
*
1979-08-10
1981-11-10
Toyota Jidosha Kogyo Kabushiki Kaisha
Polyisocyanurate resin and process for making the same
US4362678A
(en)
*
1980-01-18
1982-12-07
The Celotex Corporation
Method of making polyisocyanurate foam laminate
DE3139395C2
(en)
*
1981-10-03
1984-09-13
Bayer Ag, 5090 Leverkusen
Process for consolidating geological rock, earth and coal formations
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1982-06-01
1987-05-15
Dow Chemical Co
POLYURETHANE AND URETHANE MODIFIED ISOCYANURATE FOAMS AND A PROCESS FOR THEIR MANUFACTURE.
US4401769A
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1982-06-23
1983-08-30
Sealed Air Corporation
Foam, composition and method useful for retrofit insulation
US4425446A
(en)
1982-06-23
1984-01-10
Sealed Air Corporation
Urea-modified isocyanurate foam, composition and method
US4430840A
(en)
*
1982-06-23
1984-02-14
Sealed Air Corporation
Foam, composition and method useful for retrofit insulation
US4444913A
(en)
*
1982-11-18
1984-04-24
Thermocell Development, Ltd.
Modified polyisocyanurate foam and method of preparation
DE3309127A1
(en)
*
1983-03-15
1984-09-20
Basf Ag, 6700 Ludwigshafen
CELLED POLYURETHANE MOLDED BODIES, METHOD FOR THE PRODUCTION THEREOF BY THERMOPLASTIC DEFORMING OF POLYESTER-POLYURETHANE FOAMS AND THE USE THEREOF
US4607064A
(en)
*
1983-05-16
1986-08-19
The Dow Chemical Company
Polyurethane and urethane-modified isocyanurate foams and a polyol composition useful in their preparation
US4520042A
(en)
*
1983-06-20
1985-05-28
Thermocell Development, Ltd.
High-modulus, flexible urethane coating and method of preparation
US4661529A
(en)
*
1984-08-09
1987-04-28
The Dow Chemical Company
Polyurethane and urethane-modified isocyanurate foams and a polyol composition useful in their preparation
JPH0621147B2
(en)
*
1985-09-27
1994-03-23
三井東圧化学株式会社
Manufacturing method for rigid polyurethane foam
US4623673A
(en)
*
1985-10-24
1986-11-18
The Dow Chemical Company
Urethane-modified polyisocyanurate rigid foam
DE3610961A1
(en)
*
1986-04-02
1987-10-08
Bayer Ag
THERMALLY DEFORMABLE PUR HARD FOAM, A METHOD FOR THE PRODUCTION THEREOF AND THEIR USE FOR THE PRODUCTION OF INTERIOR CAR LINING
DE3737524C2
(en)
*
1987-11-05
1994-12-22
Bayer Ag
Process for the production of ski cores
DE3942468A1
(en)
*
1989-12-22
1991-06-27
Bayer Ag
METHOD FOR THE PRODUCTION OF MOLDED BODIES OR FILMS FROM CROSS-LINKED POLYISOCYANATE-POLYADDITION PRODUCTS AND THE MOLDED BODIES OBTAINED THEREFORE
US5251849A
(en)
*
1989-12-26
1993-10-12
Florida International University For Board Of Regents
Strain reduced airplane skin
DE4001249A1
(en)
*
1990-01-18
1991-07-25
Bayer Ag
Cold formable open cell rigid polyurethane foam prodn. – from specified poly:ol component and crude MDI, used for car canopy
CA2071030A1
(en)
*
1991-06-17
1992-12-18
Kenneth P. Klapper
Thermoformable polyisocyanurate foam laminates for interior finishing applications
US5260344A
(en)
*
1992-03-13
1993-11-09
Asahi Glass Company, Ltd.
Open cell rigid isocyanurate foams and method for producing the same and vacuum heat insulating layer by use of the same
FR2737433B1
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*
1995-08-02
1997-10-31
Maillet Orthopedie Sarl
METHOD OF MANUFACTURING BY MOLDING A SEAT IN PARTICULAR OF AN ORTHOPEDIC SEAT AND SEAT OBTAINED
US6723761B1
(en)
*
1996-02-15
2004-04-20
Bose Corporation
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US6722611B1
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1999-09-20
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Kuang-Hsi Wu
Reinforced aircraft skin and method
JP2002155125A
(en)
*
2000-11-20
2002-05-28
Sumika Bayer Urethane Kk
Process for producing polyurethane-modified polyisocyanurate foam
JP2004516369A
(en)
2000-12-27
2004-06-03
ワールド・プロパティーズ・インコーポレイテッド
Polyurethane foam and method for producing the same
US6990754B2
(en)
2002-08-05
2006-01-31
R. G. Barry Corporation
Slipper insole, slipper, and method for manufacturing a slipper
US6931763B2
(en)
*
2002-08-05
2005-08-23
R.G. Barry Corporation
Slipper insole, slipper, and method for manufacturing a slipper
PL1631606T3
(en)
2003-06-12
2011-11-30
Huntsman Int Llc
Process for preparing a polyisocyanurate polyurethane material
US7238730B2
(en)
*
2003-06-26
2007-07-03
Basf Corporation
Viscoelastic polyurethane foam
US7208531B2
(en)
*
2003-06-26
2007-04-24
Basf Corporation
Viscoelastic polyurethane foam
US20040266900A1
(en)
2003-06-26
2004-12-30
Raymond Neff
Viscoelastic polyurethane foam
US20070033835A1
(en)
*
2005-08-02
2007-02-15
Bray Walter T Jr
Insole arrangement; footwear with insole arrangement; and, method of preparation
CN101283012B
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*
2005-10-13
2011-07-06
亨茨曼国际有限公司
Process for preparing polyisocyanurate polyurethane material
JP5044560B2
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*
2005-10-13
2012-10-10
ハンツマン・インターナショナル・エルエルシー
Method for preparing polyisocyanurate polyurethane material
US20090005517A1
(en)
*
2006-02-21
2009-01-01
Huntsman International Llc
Process for Making a Polyisocyanurate Composite
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2006-06-14
2009-12-31
Huntsman Int Llc
sandwich panel
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2007-07-11
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Bayer MaterialScience AG
Method for drying foams made of aqueous PUR dispersions
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株式会社東洋クオリティワン
Sound absorbing shock absorber and method for manufacturing the same
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2012-09-20
2014-03-26
吴江市天源塑胶有限公司
Preparation method of high-temperature-resistant modified polyisocyanurate foamed plastic
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*
2018-08-08
2018-12-21
浙江清优材料科技有限公司
A kind of electrical core of power battery protective materials
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2018-10-12
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BSH Hausgeräte GmbH
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1973-07-10
Upjohn Co
Cellular isocyanurate containing polymers
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(en)
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1972-07-11
Upjohn Co
Low friability polyisocyanurate foams
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Texaco Development Corporation
Preparation of isocyanurate foams using alkali metal tertiaryamino dithiocarbamate salt catalysts
1976
1976-02-24
DE
DE2607380A
patent/DE2607380C3/en
not_active
Expired
1977
1977-02-04
US
US05/765,490
patent/US4129697A/en
not_active
Expired – Lifetime
1977-02-17
BR
BR7700994A
patent/BR7700994A/en
unknown
1977-02-22
GB
GB7340/77A
patent/GB1517673A/en
not_active
Expired
1977-02-22
IT
IT48157/77A
patent/IT1083472B/en
active
1977-02-22
BE
BE175147A
patent/BE851698A/en
not_active
IP Right Cessation
1977-02-23
SE
SE7702008A
patent/SE434161B/en
not_active
IP Right Cessation
1977-02-23
ES
ES456177A
patent/ES456177A1/en
not_active
Expired
1977-02-23
NL
NL7701943A
patent/NL7701943A/en
not_active
Application Discontinuation
1977-02-24
JP
JP1874877A
patent/JPS52103495A/en
active
Granted
Cited By (1)
* Cited by examiner, † Cited by third party
Publication number
Priority date
Publication date
Assignee
Title
GB2249793A
(en)
*
1990-11-16
1992-05-20
Basf Corp
Integral-skin rigid urethane foam
Also Published As
Publication number
Publication date
DE2607380A1
(en)
1977-08-25
NL7701943A
(en)
1977-08-26
JPS52103495A
(en)
1977-08-30
IT1083472B
(en)
1985-05-21
ES456177A1
(en)
1978-01-16
DE2607380C3
(en)
1981-07-23
BE851698A
(en)
1977-08-22
JPS546280B2
(en)
1979-03-27
SE434161B
(en)
1984-07-09
DE2607380B2
(en)
1980-09-18
SE7702008L
(en)
1977-08-25
BR7700994A
(en)
1977-10-18
US4129697A
(en)
1978-12-12
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Legal Events
Date
Code
Title
Description
1978-11-15
PS
Patent sealed [section 19, patents act 1949]
1992-10-21
PCNP
Patent ceased through non-payment of renewal fee
