GB1149560A

GB1149560A – Improvements in refrigeration process
– Google Patents

GB1149560A – Improvements in refrigeration process
– Google Patents
Improvements in refrigeration process

Info

Publication number
GB1149560A

GB1149560A
GB57403/66A
GB5740366A
GB1149560A
GB 1149560 A
GB1149560 A
GB 1149560A
GB 57403/66 A
GB57403/66 A
GB 57403/66A
GB 5740366 A
GB5740366 A
GB 5740366A
GB 1149560 A
GB1149560 A
GB 1149560A
Authority
GB
United Kingdom
Prior art keywords
passed
helium
valve
liquid
chamber
Prior art date
1965-12-28
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB57403/66A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Air Products and Chemicals Inc

Original Assignee
Air Products and Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1965-12-28
Filing date
1966-12-22
Publication date
1969-04-23

1966-12-22
Application filed by Air Products and Chemicals Inc
filed
Critical
Air Products and Chemicals Inc

1969-04-23
Publication of GB1149560A
publication
Critical
patent/GB1149560A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

238000000034
method
Methods

0.000
title
abstract
4

238000005057
refrigeration
Methods

0.000
title
abstract
2

239000001307
helium
Substances

0.000
abstract
9

229910052734
helium
Inorganic materials

0.000
abstract
9

SWQJXJOGLNCZEY-UHFFFAOYSA-N
helium atom
Chemical compound

[He]
SWQJXJOGLNCZEY-UHFFFAOYSA-N
0.000
abstract
9

IJGRMHOSHXDMSA-UHFFFAOYSA-N
Atomic nitrogen
Chemical compound

N#N
IJGRMHOSHXDMSA-UHFFFAOYSA-N
0.000
abstract
8

239000007788
liquid
Substances

0.000
abstract
7

229910052757
nitrogen
Inorganic materials

0.000
abstract
4

230000006835
compression
Effects

0.000
abstract
3

238000007906
compression
Methods

0.000
abstract
3

239000007789
gas
Substances

0.000
abstract
3

238000001816
cooling
Methods

0.000
abstract
1

239000000203
mixture
Substances

0.000
abstract
1

239000000126
substance
Substances

0.000
abstract
1

Classifications

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/02—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process

F25J1/0243—Start-up or control of the process; Details of the apparatus used; Details of the refrigerant compression system used

F25J1/0257—Construction and layout of liquefaction equipments, e.g. valves, machines

F25J1/0275—Construction and layout of liquefaction equipments, e.g. valves, machines adapted for special use of the liquefaction unit, e.g. portable or transportable devices

F25J1/0276—Laboratory or other miniature devices

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25B—REFRIGERATION MACHINES, PLANTS OR SYSTEMS; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS

F25B9/00—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point

F25B9/002—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point characterised by the refrigerant

F25B9/004—Compression machines, plants or systems, in which the refrigerant is air or other gas of low boiling point characterised by the refrigerant the refrigerant being air

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/0002—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the fluid to be liquefied

F25J1/0005—Light or noble gases

F25J1/0007—Helium

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production

F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration»

F25J1/0035—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration» by gas expansion with extraction of work

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production

F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration»

F25J1/0035—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration» by gas expansion with extraction of work

F25J1/0037—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration» by gas expansion with extraction of work of a return stream

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/003—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production

F25J1/0032—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration»

F25J1/004—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. «internal refrigeration» by flash gas recovery

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/02—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process

F25J1/0221—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using the cold stored in an external cryogenic component in an open refrigeration loop

F25J1/0224—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using the cold stored in an external cryogenic component in an open refrigeration loop in combination with an internal quasi-closed refrigeration loop

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J1/00—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures

F25J1/02—Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process

F25J1/0228—Coupling of the liquefaction unit to other units or processes, so-called integrated processes

F25J1/0235—Heat exchange integration

F25J1/0236—Heat exchange integration providing refrigeration for different processes treating not the same feed stream

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J2210/00—Processes characterised by the type or other details of the feed stream

F25J2210/42—Nitrogen

F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING

F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES

F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE

F25J2270/00—Refrigeration techniques used

F25J2270/90—External refrigeration, e.g. conventional closed-loop mechanical refrigeration unit using Freon or NH3, unspecified external refrigeration

F25J2270/912—Liquefaction cycle of a low-boiling (feed) gas in a cryocooler, i.e. in a closed-loop refrigerator

Abstract

1,149,560. Refrigerating; gas liquefaction process. AIR PRODUCTS & CHEMICALS Inc. 22 Dec., 1966 [28 Dec., 1965], No. 57403/66. Heading F4H and F4P. In a refrigeration process, compressed helium is cooled by heat exchange, expanded in an expansion engine without liquefaction and further expanded by Joule- Thomson expansion so as at least partially to liquefy. As illustrated, helium is compressed in stages 12, 15 and 17 and passed through heat exchanger 21, liquid nitrogen bath 78, and heat exchangers 28 and 31 to a reciprocating or turbine type expansion engine 33. The discharge pressure of the engine is above the critical pressure of helium. Gas from the engine passes directly to a Joule- Thomson valve 35 and partially liquefied gas is passed into a phase separator 37. Liquid helium may be withdrawn from the system through a line controlled by a valve 38. Vapour from the separator 37 may, by closing a valve 39 and opening valve 40 and 41, be passed through a coil 44 to cool a chamber 45 and then be passed through the shell spaces of heat exchangers 31, 28 and 22 to the input of compressor stage 12. By closing the valves 40 and 41, and opening the valve 39, the vapour may be passed direct to the shell spaces. If product liquid helium is not required, the valve 38 may be closed and a mixture of vapour and liquid passed to the chamber 45. The heat exchanger 28 is cooled by a compression circuit including a compressor 55 drawing helium from the compressor stage 17 and passing it through a heat exchanger 58, the nitrogen bath 78 and a heat exchanger 69 to an expansion turbine 65. Helium from the turbine is passed through heat exchangers 28, 69 and 58 to be returned to a point between the compressor stages 12 and 15. The illustrated compression circuit may be replaced by an independent circuit. The colder components of the system are contained within a chamber 73 and liquid nitrogen from a source is passed through the walls of the chamber to the bath 78. Vapourized nitrogen from the bath 78 passes through heat exchangers 22 and 58 to an exhaust 86. Valves 90 and 91 are controlled in accordance with the amount of liquid helium withdrawn from the process so that the cooling power of the compression circuit increases with the amount of liquid helium required. Preferred operating conditions are disclosed.

GB57403/66A
1965-12-28
1966-12-22
Improvements in refrigeration process

Expired

GB1149560A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US516887A

US3377811A
(en)

1965-12-28
1965-12-28
Liquefaction process employing expanded feed as refrigerant

Publications (1)

Publication Number
Publication Date

GB1149560A
true

GB1149560A
(en)

1969-04-23

Family
ID=24057500
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB57403/66A
Expired

GB1149560A
(en)

1965-12-28
1966-12-22
Improvements in refrigeration process

Country Status (2)

Country
Link

US
(1)

US3377811A
(en)

GB
(1)

GB1149560A
(en)

Families Citing this family (8)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

CH527398A
(en)

*

1966-04-01
1972-08-31
Nautchno Izsledovatelski Sekto
Liquefaction of neon with turboexpander

BE758567A
(en)

*

1969-11-07
1971-05-06
Fluor Corp

LOW PRESSURE ETHYLENE RECOVERY PROCESS

US7732953B2
(en)

*

2007-06-12
2010-06-08
Hamilton Sundstrand Corporation
Electric motor cooling

FR2919716B1
(en)

*

2007-07-31
2014-12-19
Air Liquide

LOW TEMPERATURE COOLING METHOD AND USE THEREOF

FR2980564A1
(en)

*

2011-09-23
2013-03-29
Air Liquide

REFRIGERATION METHOD AND INSTALLATION

CN103411386B
(en)

*

2013-07-25
2015-05-13
杭州求是透平机制造有限公司
Freezing expansion type chlorine liquefying method

DE102015009255A1
(en)

*

2015-07-16
2017-01-19
Linde Aktiengesellschaft

Method for cooling a process stream

US10808967B2
(en)

*

2017-01-16
2020-10-20
Praxair Technology, Inc.
Refrigeration cycle for liquid oxygen densification

Family Cites Families (7)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US2909903A
(en)

*

1956-11-07
1959-10-27
Little Inc A
Liquefaction of low-boiling gases

US2954677A
(en)

*

1956-12-07
1960-10-04
Air Liquide
Gas liquefaction process

DE1040575B
(en)

*

1957-06-22
1958-10-09
Linde Eismasch Ag

Method for operating regenerators, preferably for use in the low temperature range

US2932173A
(en)

*

1957-12-13
1960-04-12
Beech Aircraft Corp
Method of liquefying helium

SU145251A1
(en)

*

1961-04-01
1961-11-30
А.Г. Зельдович

Method for hydrogen liquefaction

NL135362C
(en)

*

1963-09-06

US3250079A
(en)

*

1965-03-15
1966-05-10
Little Inc A
Cryogenic liquefying-refrigerating method and apparatus

1965

1965-12-28
US
US516887A
patent/US3377811A/en
not_active
Expired – Lifetime

1966

1966-12-22
GB
GB57403/66A
patent/GB1149560A/en
not_active
Expired

Also Published As

Publication number
Publication date

US3377811A
(en)

1968-04-16

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