GB1267575A

GB1267575A – Preparation of synthetic mullite
– Google Patents

GB1267575A – Preparation of synthetic mullite
– Google Patents
Preparation of synthetic mullite

Info

Publication number
GB1267575A

GB1267575A
GB46416/69A
GB4641669A
GB1267575A
GB 1267575 A
GB1267575 A
GB 1267575A
GB 46416/69 A
GB46416/69 A
GB 46416/69A
GB 4641669 A
GB4641669 A
GB 4641669A
GB 1267575 A
GB1267575 A
GB 1267575A
Authority
GB
United Kingdom
Prior art keywords
solution
aluminium
silicate
silica
alumina
Prior art date
1968-12-16
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB46416/69A
Inventor
Clark Ace Rundell
John Anthony Kwedar
Heyman Clarke Duecker
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

WR Grace and Co

Original Assignee
WR Grace and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1968-12-16
Filing date
1969-09-19
Publication date
1972-03-22

1969-09-19
Application filed by WR Grace and Co
filed
Critical
WR Grace and Co

1972-03-22
Publication of GB1267575A
publication
Critical
patent/GB1267575A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B33/00—Silicon; Compounds thereof

C01B33/20—Silicates

C01B33/36—Silicates having base-exchange properties but not having molecular sieve properties

C01B33/38—Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type

C01B33/42—Micas ; Interstratified clay-mica products

B—PERFORMING OPERATIONS; TRANSPORTING

B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL

B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS

B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium

B01J21/16—Clays or other mineral silicates

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B33/00—Silicon; Compounds thereof

C01B33/20—Silicates

C01B33/26—Aluminium-containing silicates, i.e. silico-aluminates

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B33/00—Silicon; Compounds thereof

C01B33/20—Silicates

C01B33/36—Silicates having base-exchange properties but not having molecular sieve properties

C01B33/38—Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type

C01B33/40—Clays

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B33/00—Silicon; Compounds thereof

C01B33/20—Silicates

C01B33/36—Silicates having base-exchange properties but not having molecular sieve properties

C01B33/46—Amorphous silicates, e.g. so-called «amorphous zeolites»

Abstract

1,267,575. Mullite synthesis. W. R. GRACE & CO. 19 Sept., 1969 [16 Dec., 1968], No. 46416/67. Heading C1A. Mullite is synthesized by mixing a solution of an alkali metal silicate or a sol of silica and a solution of an aluminate or aluminium salt, at a pH sufficient to form a gel of silica and alumina, which is spray-dried, washed and calcined, e.g. at 900-1400‹ C. The solution of a silicate is preferably sodium silicate. The aluminium compound is preferably an inorganic aluminium salt, such as aluminium nitrate. Example 1 uses a solution of sodium silicate and sodium hydroxide as the silica source and a solution of alumina trihydrate and sodium hydroxide, mixed with a solution of aluminium nitrate as the alumina source. The sodium content of the spray-dried product may be reduced by ion exchangewith ammonium sulphate solution. The product may have a surface area of up to 120 m2/g.

GB46416/69A
1968-12-16
1969-09-19
Preparation of synthetic mullite

Expired

GB1267575A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US78424368A

1968-12-16
1968-12-16

Publications (1)

Publication Number
Publication Date

GB1267575A
true

GB1267575A
(en)

1972-03-22

Family
ID=25131806
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB46416/69A
Expired

GB1267575A
(en)

1968-12-16
1969-09-19
Preparation of synthetic mullite

Country Status (5)

Country
Link

US
(1)

US3533738A
(en)

CA
(1)

CA928935A
(en)

DE
(1)

DE1952575A1
(en)

FR
(1)

FR2026196A1
(en)

GB
(1)

GB1267575A
(en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US3951677A
(en)

*

1970-09-04
1976-04-20
Howard Wayne Jacobson
Mullite fibrils

US3993499A
(en)

*

1974-10-04
1976-11-23
E. I. Du Pont De Nemours And Company
Process for producing a particulate mullite fibril containing composition

JPS59190983A
(en)

*

1983-04-12
1984-10-29
Mitsubishi Petrochem Co Ltd
Filler for using in reactor for preparation of ethylene oxide

IT1187668B
(en)

*

1985-05-16
1987-12-23
Montefluos Spa

PROCEDURE FOR OBTAINING GRANULAR SODIUM PERBORATE WITH A GOOD MECHANICAL RESISTANCE

JPH0611667B2
(en)

*

1985-05-30
1994-02-16
工業技術院長

Method for producing alumina-silica ceramics sintered body having excellent high temperature strength

JPS61281013A
(en)

*

1985-06-05
1986-12-11
Chichibu Cement Co Ltd
Production of mullite powder of high purity

JPS6217005A
(en)

*

1985-07-15
1987-01-26
Showa Denko Kk
Preparation of mullite powder having high purity

US5085705A
(en)

*

1989-01-12
1992-02-04
J. M. Huber Corporation
Alumina-silica-sulfates, method of preparation and compositions

US5030284A
(en)

*

1989-01-12
1991-07-09
Withiam Michael C
Alumina-silica-sulfate compositions

US5478785A
(en)

*

1989-11-06
1995-12-26
Pennsylvania Research Corporation
Infiltration process for introducing additional phases for multiphase (composite) materials

FR2655971B1
(en)

*

1989-12-18
1992-04-17
Hoechst France

PROCESS FOR OBTAINING REFRACTORY METAL OXIDES BASED ON SILICA BY SOL-GEL ROUTE IN AQUEOUS MEDIUM.

US11208514B2
(en)

2008-03-20
2021-12-28
Chevron Phillips Chemical Company Lp
Silica-coated alumina activator-supports for metallocene catalyst compositions

US20090240010A1
(en)

*

2008-03-20
2009-09-24
Mcdaniel Max P
Alumina-silica activator-supports for metallocene catalyst compositions

US7884163B2
(en)

2008-03-20
2011-02-08
Chevron Phillips Chemical Company Lp
Silica-coated alumina activator-supports for metallocene catalyst compositions

US8937139B2
(en)

2012-10-25
2015-01-20
Chevron Phillips Chemical Company Lp
Catalyst compositions and methods of making and using same

US8895679B2
(en)

2012-10-25
2014-11-25
Chevron Phillips Chemical Company Lp
Catalyst compositions and methods of making and using same

US9034991B2
(en)

2013-01-29
2015-05-19
Chevron Phillips Chemical Company Lp
Polymer compositions and methods of making and using same

US8877672B2
(en)

2013-01-29
2014-11-04
Chevron Phillips Chemical Company Lp
Catalyst compositions and methods of making and using same

CN108383132B
(en)

*

2018-03-19
2021-07-16
华南理工大学
Low-temperature preparation method of superfine mullite powder

Family Cites Families (9)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US1741920A
(en)

*

1926-12-21
1929-12-31
Vitrefax Company
Refractory composition and method of making

US2232727A
(en)

*

1938-03-15
1941-02-25
Houdry Process Corp
Reaction of solutions

US2428895A
(en)

*

1944-07-26
1947-10-14
Davison Chemical Corp
Method of making silica containing gels

US2678282A
(en)

*

1950-06-01
1954-05-11
Pilkington Brothers Ltd
Process for manufacturing synthetic inorganic silicates or the like

US2688003A
(en)

*

1951-05-14
1954-08-31
Shell Dev
Preparation of spheroidal silica alumina catalyst

DE1068232B
(en)

*

1958-01-16
1959-11-05
Farbenfabriken Bayer Aktiengesellschaft, Leverkusen-Bayerwerk

Process for the production of aluminosifficate gels

US3366445A
(en)

*

1964-02-26
1968-01-30
Harbison Walker Refractories
Mullite production

US3459501A
(en)

*

1964-10-30
1969-08-05
Mobil Oil Corp
Method for preparing high-silica faujasite

US3460904A
(en)

*

1968-01-15
1969-08-12
Union Oil Co
Process for the manufacture of metalcation-deficient zeolites

1968

1968-12-16
US
US784243A
patent/US3533738A/en
not_active
Expired – Lifetime

1969

1969-09-16
CA
CA062094A
patent/CA928935A/en
not_active
Expired

1969-09-19
GB
GB46416/69A
patent/GB1267575A/en
not_active
Expired

1969-10-17
FR
FR6935713A
patent/FR2026196A1/fr
not_active
Withdrawn

1969-10-18
DE
DE19691952575
patent/DE1952575A1/en
active
Pending

Also Published As

Publication number
Publication date

US3533738A
(en)

1970-10-13

FR2026196A1
(en)

1970-09-18

DE1952575A1
(en)

1970-09-03

CA928935A
(en)

1973-06-26

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(en)

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