GB1360587A

GB1360587A – Process for the purification of titanium tetrachloride
– Google Patents

GB1360587A – Process for the purification of titanium tetrachloride
– Google Patents
Process for the purification of titanium tetrachloride

Info

Publication number
GB1360587A

GB1360587A
GB5411872A
GB5411872A
GB1360587A
GB 1360587 A
GB1360587 A
GB 1360587A
GB 5411872 A
GB5411872 A
GB 5411872A
GB 5411872 A
GB5411872 A
GB 5411872A
GB 1360587 A
GB1360587 A
GB 1360587A
Authority
GB
United Kingdom
Prior art keywords
ticl
agent
support
tio
purifying
Prior art date
1971-12-27
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB5411872A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Societa Italiana Resine SpA SIR

Original Assignee
Societa Italiana Resine SpA SIR
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1971-12-27
Filing date
1972-11-22
Publication date
1974-07-17

1971-12-27
Priority claimed from IT3295571A
external-priority
patent/IT951960B/en

1972-05-03
Priority claimed from IT2384972A
external-priority
patent/IT1007507B/en

1972-11-22
Application filed by Societa Italiana Resine SpA SIR
filed
Critical
Societa Italiana Resine SpA SIR

1974-07-17
Publication of GB1360587A
publication
Critical
patent/GB1360587A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS

C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS

C22B34/00—Obtaining refractory metals

C22B34/10—Obtaining titanium, zirconium or hafnium

C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 – C01G23/08

C22B34/1218—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 – C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes

C22B34/1231—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 – C01G23/08 obtaining titanium or titanium compounds from ores or scrap by dry processes treatment or purification of titanium containing products obtained by dry processes, e.g. condensation

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F

C01G23/00—Compounds of titanium

C01G23/02—Halides of titanium

C01G23/022—Titanium tetrachloride

C01G23/024—Purification of tetrachloride

Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS

Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE

Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS

Y02P10/00—Technologies related to metal processing

Y02P10/20—Recycling

Abstract

1360587 Purifying TiCl 4 SOC ITALIANA RESINE SIR SpA 22 Nov 1972 [27 Dec 1971 3 May 1972] 54118/72 Heading C1A TiCl 4 is purified by contact with Na which has been deposited on an inert granular support selected from SiO 2 , Al 2 O 3 , TiO 2 , ZnO, KgO, alkaline earth metal salts, NaCl, KCl, diatomaceous earth, pumice, asbestos, bauxite, quartz, aluminosilicates, silicates, polyethylene, polypropylene, porcelain, glass and active carbon. Liquid TiCl 4 may be mixed with the purifying agent and heated to 80-90‹ C. or may be percolated through a column of the agent at 50-90‹ C., and may then be distilled. Gaseous TiCl 4 , optionally diluted with N 2 , may be contacted at above 100‹ C., e.g. 110-170‹ C., with the agent in the form of a fluidized, fixed or movable bed, and may then be condensed. The agent may be prepared by melting Na in a closed vessel containing the support, heating and agitating, then slowly cooling with agitation. The support may have a size of 0À05-1 mm. and a surface area of 105 or 2À5 m.2/g. The TiCl 4 is obtained by chlorination of TiO 2 -containing materials, e.g. rutile or ilmenite ores or ilmenite slag, in the presence of carbon, and contains V as impurity.

GB5411872A
1971-12-27
1972-11-22
Process for the purification of titanium tetrachloride

Expired

GB1360587A
(en)

Applications Claiming Priority (2)

Application Number
Priority Date
Filing Date
Title

IT3295571A

IT951960B
(en)

1971-12-27
1971-12-27

PROCEDURE FOR THE PURIFICATION OF TITANIUM TETRACLORUR

IT2384972A

IT1007507B
(en)

1972-05-03
1972-05-03

PERFECTED PROCESS FOR THE PURIFICATION OF TITANIUM TETRA CHLORIDE

Publications (1)

Publication Number
Publication Date

GB1360587A
true

GB1360587A
(en)

1974-07-17

Family
ID=26328429
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB5411872A
Expired

GB1360587A
(en)

1971-12-27
1972-11-22
Process for the purification of titanium tetrachloride

Country Status (9)

Country
Link

US
(1)

US3939244A
(en)

JP
(1)

JPS5127440B2
(en)

CA
(1)

CA987883A
(en)

CH
(1)

CH557301A
(en)

DE
(1)

DE2262155A1
(en)

FR
(1)

FR2165949B1
(en)

GB
(1)

GB1360587A
(en)

NL
(1)

NL7217649A
(en)

YU
(1)

YU35613B
(en)

Families Citing this family (9)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

JPS6114134A
(en)

*

1984-06-30
1986-01-22
Hiroshi Ishizuka
Method for purifying titanium tetrachloride

DE3623322A1
(en)

*

1986-07-11
1988-01-21
Bayer Ag

METHOD FOR PRODUCING TICL (DOWN ARROW) 4 (DOWN ARROW)

US6770254B2
(en)

*

2002-01-17
2004-08-03
Air Products And Chemicals, Inc.
Purification of group IVb metal halides

WO2006054505A1
(en)

*

2004-11-16
2006-05-26
Mitsubishi Plastics, Inc.
Reflective film and reflector plate

US20060228292A1
(en)

*

2005-04-11
2006-10-12
Cronin James T
Process for purifying titanium chloride-containing feedstock

US7368096B2
(en)

*

2005-06-07
2008-05-06
E.I. Du Pont De Nemours And Company
Process for separating solids from a purification purge stream

EP2452920A1
(en)

*

2010-11-12
2012-05-16
Borealis AG
A method for recovering transition metal tetrahalide and hydrocarbons from a waste stream

US20130280149A1
(en)

*

2012-04-20
2013-10-24
Cristal Usa Inc.
Purification of Titanium Tetrachloride

CN107352567B
(en)

*

2016-05-09
2019-10-18
青海大学
The method that vacuum reduction distilation prepares high purity aluminium oxide

Family Cites Families (11)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US1796265A
(en)

*

1926-08-23
1931-03-10
Degussa
Process of manufacture of alkali-metal hydrides

US2224061A
(en)

*

1938-10-27
1940-12-03
Pittsburgh Plate Glass Co
Decolorizing titanium tetrachloride

US2396458A
(en)

*

1944-09-26
1946-03-12
Nat Lead Co
Method for the purification of titanium tetrachloride

US2530735A
(en)

*

1946-04-12
1950-11-21
Du Pont
Purification of titanium halides

GB674315A
(en)

*

1949-11-25
1952-06-18
Titan Co Inc
Method for the purification of titanium tetrachloride

US2754255A
(en)

*

1952-05-27
1956-07-10
Nat Lead Co
Decolorizing titanium tetrachloride

FR1133956A
(en)

*

1954-06-18
1957-04-04
Laporte Titanium Ltd

Process for the purification of titanium tetrahalides or zirconium tetrahalides

US2958574A
(en)

*

1955-12-02
1960-11-01
Nat Distillers Chem Corp
Purification of titanium tetrachloride

GB868851A
(en)

*

1956-09-25
1961-05-25
Laporte Titanium Ltd
Process for the purification of titanium tetrachloride

US3009772A
(en)

*

1956-09-25
1961-11-21
Laporte Titanium Ltd
Process for the purificaton of titanium tetrachloride

US3533734A
(en)

*

1968-05-09
1970-10-13
Du Pont
Purifying crude ticl4 vapor

1972

1972-11-22
GB
GB5411872A
patent/GB1360587A/en
not_active
Expired

1972-11-27
US
US05/309,828
patent/US3939244A/en
not_active
Expired – Lifetime

1972-12-14
FR
FR7244582A
patent/FR2165949B1/fr
not_active
Expired

1972-12-19
DE
DE2262155A
patent/DE2262155A1/en
active
Pending

1972-12-21
CA
CA159,679A
patent/CA987883A/en
not_active
Expired

1972-12-21
CH
CH1865372A
patent/CH557301A/en
not_active
IP Right Cessation

1972-12-25
YU
YU3228/72A
patent/YU35613B/en
unknown

1972-12-26
JP
JP47129650A
patent/JPS5127440B2/ja
not_active
Expired

1972-12-27
NL
NL7217649A
patent/NL7217649A/xx
unknown

Also Published As

Publication number
Publication date

JPS5127440B2
(en)

1976-08-12

FR2165949A1
(en)

1973-08-10

CA987883A
(en)

1976-04-27

YU35613B
(en)

1981-04-30

FR2165949B1
(en)

1975-01-03

DE2262155A1
(en)

1973-07-05

CH557301A
(en)

1974-12-31

YU322872A
(en)

1980-10-31

US3939244A
(en)

1976-02-17

JPS4878092A
(en)

1973-10-19

NL7217649A
(en)

1973-06-29

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(en)

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1975

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(en)

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Production of magnesium chloride hexahydrate

SU136567A1
(en)

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The method of refining aluminum from impurities by distillation

GB1046140A
(en)

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Method of preventing solid chloride deposition

SU684000A1
(en)

1979-09-05

Method of purifying aluminium chloride melt from ferric chloride and titanium tetrachloride

Legal Events

Date
Code
Title
Description

1974-11-27
PS
Patent sealed [section 19, patents act 1949]

1977-04-27
435
Patent endorsed ‘licences of right’ on the date specified (sect. 35/1949)

1984-08-01
PCNP
Patent ceased through non-payment of renewal fee

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