GB1459909A

GB1459909A – Device for automatic analysis by mass spectrometry
– Google Patents

GB1459909A – Device for automatic analysis by mass spectrometry
– Google Patents
Device for automatic analysis by mass spectrometry

Info

Publication number
GB1459909A

GB1459909A
GB4048474A
GB4048474A
GB1459909A
GB 1459909 A
GB1459909 A
GB 1459909A
GB 4048474 A
GB4048474 A
GB 4048474A
GB 4048474 A
GB4048474 A
GB 4048474A
GB 1459909 A
GB1459909 A
GB 1459909A
Authority
GB
United Kingdom
Prior art keywords
valve
pipe
pipes
cell
traced
Prior art date
1973-09-25
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB4048474A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

RECH ET DACTIVITES PETROLIERES

Original Assignee
RECH ET DACTIVITES PETROLIERES
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1973-09-25
Filing date
1974-09-17
Publication date
1976-12-31

1974-09-17
Application filed by RECH ET DACTIVITES PETROLIERES
filed
Critical
RECH ET DACTIVITES PETROLIERES

1976-12-31
Publication of GB1459909A
publication
Critical
patent/GB1459909A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

G—PHYSICS

G01—MEASURING; TESTING

G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

G01N1/00—Sampling; Preparing specimens for investigation

G01N1/02—Devices for withdrawing samples

G01N1/10—Devices for withdrawing samples in the liquid or fluent state

G01N1/20—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials

G01N1/2035—Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials by deviating part of a fluid stream, e.g. by drawing-off or tapping

H—ELECTRICITY

H01—ELECTRIC ELEMENTS

H01J—ELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS

H01J49/00—Particle spectrometers or separator tubes

H01J49/02—Details

H01J49/04—Arrangements for introducing or extracting samples to be analysed, e.g. vacuum locks; Arrangements for external adjustment of electron- or ion-optical components

G—PHYSICS

G01—MEASURING; TESTING

G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES

G01N1/00—Sampling; Preparing specimens for investigation

G01N1/02—Devices for withdrawing samples

G01N1/10—Devices for withdrawing samples in the liquid or fluent state

G01N2001/1031—Sampling from special places

G01N2001/1037—Sampling from special places from an enclosure (hazardous waste, radioactive)

Abstract

1459909 Automatic analysis of flowing twophase mixtures ENTREPRISE DE RECHERCHES ET D’ACTIVITES PETROLIERES ELF 17 Sept 1974 [25 Sept 1973] 40484/74 Heading G1B A device for automatic analysis by mass spectrometry of two-phase mixtures which flow continuously through main pipes 2, 4 in for example a cracking plant comprises pipes 18, 22 &c. constituting a plurality of primary loops Bi (B 1 , B 2 shown), each of the primary loops being connected to a different one of the main pipes and to a recycling circuit in the direction of 27, each loop being fitted with a flow regulating valve 6, 10 and a flowmeter 8, 12 in series, the primary loops being traced, pipes Ti each connecting a branch point in a primary loop Bi to a pneumatic valve Vj (30 as shown) through a dust filter 26, 28 and a needle valve 32, 34 for regulating the flow-rate, the pneumatic valve(s) each for operably connecting one of the pipes Ti to one end of a further traced pipe T’, a sampling cell 40 at the other end of pipe T’, a sampling pipe T» for connecting one outlet of the cell 40 to the recycle circuit through a delivery valve V’ and a flowmeter 42 in series, means 46 for measuring the pressure in the cell 40, means for regulating the pressure in the cell by regulating the opening of valve V’ in response to a difference in pressure between the pressure measured by 46 and a reference pressure, a further traced pipe for connecting cell 40 to a further pneumatic valve V», a traced capillary tube T»‘ for connecting valve V» to a chamber E, pumping means 58, 60 for creating a vacuum within chamber E, a pipe for connecting chamber E to the ionization chamber 62 of a mass spectrometer, electronic means (not shown) for simultaneously initiating the application of voltage to the acceleration electrodes of the mass spectrometer and the opening of the pneumatic valve V», and means for initiating the selective opening of the valves Vj. The pipe «tracing» may comprise electrical resistance heating wire or a steam-fed copper pipe wound around the pipe to be traced, or a steam-fed sleeve concentric with the pipe. Fig. 3 (not shown) relates to the arrangement of eight pneumatic valves connectable in series, each valve having an inlet connected to one of a series of eight pipes carrying mixture to be analyzed, the valves being selectively operated by respective pairs of electrovalves, each pair of electrovalves being operable to connect one of the two inputs of the valve to the valve output.

GB4048474A
1973-09-25
1974-09-17
Device for automatic analysis by mass spectrometry

Expired

GB1459909A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

FR7334263A

FR2245249A5
(en)

1973-09-25
1973-09-25

Publications (1)

Publication Number
Publication Date

GB1459909A
true

GB1459909A
(en)

1976-12-31

Family
ID=9125513
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB4048474A
Expired

GB1459909A
(en)

1973-09-25
1974-09-17
Device for automatic analysis by mass spectrometry

Country Status (9)

Country
Link

US
(1)

US3943363A
(en)

JP
(1)

JPS5740975B2
(en)

BE
(1)

BE819367A
(en)

CA
(1)

CA1023472A
(en)

DE
(1)

DE2445124C3
(en)

FR
(1)

FR2245249A5
(en)

GB
(1)

GB1459909A
(en)

IT
(1)

IT1022244B
(en)

NL
(1)

NL7411676A
(en)

Families Citing this family (17)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4207465A
(en)

*

1978-07-03
1980-06-10
Phillips Petroleum Company
Isotope analysis with a mass spectrometer using small samples

US4380701A
(en)

*

1980-10-02
1983-04-19
Texaco Inc.
Nuclear well logging with neutron source and separate spaced radiation detectors to determine silicon/oxygen ratio

US4960992A
(en)

*

1983-08-30
1990-10-02
Research Corporation Technologies
Method and means for vaporizing liquids by means of heating a sample capillary tube for detection or analysis

US4814612A
(en)

*

1983-08-30
1989-03-21
Research Corporation
Method and means for vaporizing liquids for detection or analysis

US4861989A
(en)

*

1983-08-30
1989-08-29
Research Corporation Technologies, Inc.
Ion vapor source for mass spectrometry of liquids

US4722830A
(en)

*

1986-05-05
1988-02-02
General Electric Company
Automated multiple stream analysis system

US4791291A
(en)

*

1986-07-14
1988-12-13
The Dow Chemical Company
Mass spectrometer sampling system for a liquid stream

FR2645966B1
(en)

*

1989-04-18
1991-06-07
Commissariat Energie Atomique

INSTALLATION OF CONTINUOUS AND REAL-TIME MEASUREMENTS, METAL MASSES IN ACID SOLUTION, AND THE ACIDITY OF THIS SOLUTION

JP2892795B2
(en)

*

1989-09-12
1999-05-17
エーザイ株式会社

Mobile phase conversion method and apparatus in high performance liquid chromatography mass spectrometry

JPH03282252A
(en)

*

1990-03-30
1991-12-12
Hitachi Ltd
Apparatus for analyzing very minute amount of element of plasma

DE4133300C2
(en)

*

1991-10-08
1996-07-11
Fraunhofer Ges Forschung

Method and device for determining strippable substances from liquids

US5237175A
(en)

*

1992-02-26
1993-08-17
Varian Associates, Inc.
Reagent gas control for an ion trap mass spectrometer used in the chemical ionization mode

US5376335A
(en)

*

1993-04-30
1994-12-27
Gleaves; John T.
Apparatus for study and analysis of products of catalytic reaction

US6063633A
(en)

*

1996-02-28
2000-05-16
The University Of Houston
Catalyst testing process and apparatus

CN109536755B
(en)

*

2018-12-13
2020-11-27
中国兵器工业第五九研究所
Intelligent control system for air content of aluminum alloy melt

CN112657960B
(en)

*

2020-12-16
2022-11-22
华能海南发电股份有限公司电力检修分公司
One set of system of sweeping to denitration export net sampling device

CN114152475B
(en)

*

2022-02-07
2022-04-08
东营石油技术与装备产业研究院有限公司
Closed type high-efficiency sampling device for petroleum detection

Family Cites Families (2)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US2977471A
(en)

*

1958-09-25
1961-03-28
Socony Mobil Oil Co Inc
Apparatus for automatically operating a mass spectrometer

GB979958A
(en)

*

1963-06-05
1965-01-06
Exxon Research Engineering Co
Automatic computer for use with mass spectrometers

1973

1973-09-25
FR
FR7334263A
patent/FR2245249A5/fr
not_active
Expired

1974

1974-08-29
BE
BE148056A
patent/BE819367A/en
not_active
IP Right Cessation

1974-09-03
NL
NL7411676A
patent/NL7411676A/en
active
Search and Examination

1974-09-17
US
US05/506,730
patent/US3943363A/en
not_active
Expired – Lifetime

1974-09-17
GB
GB4048474A
patent/GB1459909A/en
not_active
Expired

1974-09-20
DE
DE2445124A
patent/DE2445124C3/en
not_active
Expired

1974-09-23
CA
CA209,963A
patent/CA1023472A/en
not_active
Expired

1974-09-24
IT
IT27622/74A
patent/IT1022244B/en
active

1974-09-25
JP
JP49110403A
patent/JPS5740975B2/ja
not_active
Expired

Also Published As

Publication number
Publication date

NL7411676A
(en)

1975-03-27

DE2445124B2
(en)

1978-07-20

DE2445124C3
(en)

1979-03-29

US3943363A
(en)

1976-03-09

DE2445124A1
(en)

1975-04-10

JPS5740975B2
(en)

1982-08-31

IT1022244B
(en)

1978-03-20

JPS5061286A
(en)

1975-05-26

FR2245249A5
(en)

1975-04-18

BE819367A
(en)

1974-12-16

CA1023472A
(en)

1977-12-27

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Legal Events

Date
Code
Title
Description

1977-09-21
PS
Patent sealed [section 19, patents act 1949]

1989-05-10
PCNP
Patent ceased through non-payment of renewal fee

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