GB1501461A

GB1501461A – Synthesis of open framework zeolites
– Google Patents

GB1501461A – Synthesis of open framework zeolites
– Google Patents
Synthesis of open framework zeolites

Info

Publication number
GB1501461A

GB1501461A
GB11464/75A
GB1146475A
GB1501461A
GB 1501461 A
GB1501461 A
GB 1501461A
GB 11464/75 A
GB11464/75 A
GB 11464/75A
GB 1146475 A
GB1146475 A
GB 1146475A
GB 1501461 A
GB1501461 A
GB 1501461A
Authority
GB
United Kingdom
Prior art keywords
mixture
organic template
slurry
open framework
synthesis
Prior art date
1974-03-20
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Expired

Application number
GB11464/75A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

WR Grace and Co

Original Assignee
WR Grace and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
1974-03-20
Filing date
1975-03-19
Publication date
1978-02-15

1975-03-19
Application filed by WR Grace and Co
filed
Critical
WR Grace and Co

1978-02-15
Publication of GB1501461A
publication
Critical
patent/GB1501461A/en

Status
Expired
legal-status
Critical
Current

Links

Espacenet

Global Dossier

Discuss

Classifications

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination

C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof

C01B39/14—Type A

C01B39/145—Type A using at least one organic template directing agent

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination

C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof

C01B39/04—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof using at least one organic template directing agent, e.g. an ionic quaternary ammonium compound or an aminated compound

C—CHEMISTRY; METALLURGY

C01—INORGANIC CHEMISTRY

C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C

C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination

C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof

C01B39/30—Erionite or offretite type, e.g. zeolite T

C01B39/305—Erionite or offretite type, e.g. zeolite T using at least one organic template directing agent

Abstract

1501461 Open framework zeolite preparation W R GRACE & CO 19 March 1975 [20 March 1974] 11464/75 Heading C1A A method of synthesizing an open framework zeolite comprises ageing an aqueous mixture of a source of silica and of alumina and an alkali metal hydroxide and organic template ion for 12-300 hours at 0-120 C. to form a nucleation slurry which is added to a zeolite synthesis mixture having the same components as the nucleation slurry but without the organic template ion, and effecting hydrothermal crystallization of said mixture. The organic template compounds are preferably quaternary compounds of group 5A elements, R 4 NM+A–, where R is C 1 -C 7 alkyl or aryl group. The nucleation slurry is preferably formed from a mixture of composition 2-8 Z 2 O:Al 2 O 3 :2-20 SiO 2 : 120-400 H 2 O where Z is a mixture of alkali metal oxide ion and organic template ion, and the slurry is preferably added to the synthesis mixture in a quantity of 1-20% by weight of the resultant mixture.

GB11464/75A
1974-03-20
1975-03-19
Synthesis of open framework zeolites

Expired

GB1501461A
(en)

Applications Claiming Priority (1)

Application Number
Priority Date
Filing Date
Title

US05/452,734

US3947482A
(en)

1974-03-20
1974-03-20
Method for producing open framework zeolites

Publications (1)

Publication Number
Publication Date

GB1501461A
true

GB1501461A
(en)

1978-02-15

Family
ID=23797703
Family Applications (1)

Application Number
Title
Priority Date
Filing Date

GB11464/75A
Expired

GB1501461A
(en)

1974-03-20
1975-03-19
Synthesis of open framework zeolites

Country Status (5)

Country
Link

US
(1)

US3947482A
(en)

JP
(1)

JPS5813492B2
(en)

CA
(1)

CA1038850A
(en)

DE
(1)

DE2511975A1
(en)

GB
(1)

GB1501461A
(en)

Cited By (3)

* Cited by examiner, † Cited by third party

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Publication date
Assignee
Title

CN104071802A
(en)

*

2014-07-03
2014-10-01
太原理工大学
Preparation method for hierarchical pore low-silicate zeolite

CN106542539A
(en)

*

2016-10-25
2017-03-29
浙江大学
In the method that polyquaternary ammonium salt template synthesizes 23 zeolite molecular sieves of macropore EMM

CN108862305A
(en)

*

2018-07-17
2018-11-23
武汉科技大学
A method of acid resistance OFF type adsorbent of molecular sieve is synthesized using Coaseries kaolin

Families Citing this family (48)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US4061717A
(en)

*

1974-10-03
1977-12-06
Mobil Oil Corporation
Directed crystallization of synthetic aluminosilicates

GB1567948A
(en)

*

1976-07-22
1980-05-21
Ici Ltd
Zeolite synthesis

NZ185397A
(en)

*

1976-11-04
1979-12-11
Mobil Oil Corp
Crystalline aluminosilicate zeolites and use as catalysts

US4112056A
(en)

*

1977-05-02
1978-09-05
Mobil Oil Corporation
Preparation of zeolites

US4108881A
(en)

*

1977-08-01
1978-08-22
Mobil Oil Corporation
Synthesis of zeolite ZSM-11

US4100262A
(en)

*

1977-08-15
1978-07-11
Mobil Oil Corporation
Synthesis of zeolite ZSM-5

US4173622A
(en)

*

1978-01-03
1979-11-06
Fmc Corporation
Zeolite A crystals of uniformly small particle size and the manufacture thereof

AU527116B2
(en)

*

1978-11-13
1983-02-17
Mobil Oil Corp.
Method for synthesis of zeolite zsm-5

CA1136112A
(en)

*

1979-01-05
1982-11-23
William J. Ball
Method for producing aluminosilicates, their use as catalysts and catalytic compositions containing them

US4205053A
(en)

*

1979-02-01
1980-05-27
Mobil Oil Corporation
Manufacture of nitrogenous zeolites

US4205052A
(en)

*

1979-02-01
1980-05-27
Mobil Oil Corporation
Manufacture of synthetic mordenite

US4357233A
(en)

*

1980-06-06
1982-11-02
Mobil Oil Corporation
Catalytic conversion with zeolite ZSM-39

US4310440A
(en)

*

1980-07-07
1982-01-12
Union Carbide Corporation
Crystalline metallophosphate compositions

DE3274844D1
(en)

*

1981-04-14
1987-02-05
Ici Plc
Zeolites

DE3171306D1
(en)

*

1981-05-07
1985-08-14
Mobil Oil Corp
Crystalline zeolitic material, synthesis and use thereof

JPS57191222A
(en)

*

1981-05-13
1982-11-25
Mobil Oil Corp
Crystalline zeolite substance, manufacture and conversion of organic raw material using same

DE3211433C2
(en)

*

1982-03-27
1984-12-13
Degussa Ag, 6000 Frankfurt

Crystalline aluminosilicate PZ 1 and process for its production

DE3217322A1
(en)

*

1982-05-08
1983-11-10
Hoechst Ag, 6230 Frankfurt

CRYSTALLINE ALUMINOSILICATE ZEOLITE, METHOD FOR THE PRODUCTION THEREOF AND THEIR USE

JPS5997523A
(en)

*

1982-11-24
1984-06-05
Agency Of Ind Science & Technol
Zeolite containing alkaline earth metal, its manufacture and manufacture of olefin

FR2542301B1
(en)

*

1983-03-07
1985-08-16
Centre Nat Rech Scient

PERFECTED CRYSTALLINE ALUMINOSILICATE OR PERFECTED ZEOLITE WITH THE STRUCTURE OF THE OFFERING

US4510256A
(en)

*

1983-05-13
1985-04-09
Chevron Research Company
Zeolite SSZ-19

NZ208048A
(en)

*

1983-05-26
1986-10-08
Mobil Oil Corp
Method for synthesising zeolites,incorporating alumina source of limited solubility

US4554146A
(en)

*

1983-11-10
1985-11-19
Exxon Research And Engineering Co.
Process for preparing a zeolite of the L type using organic templates

CA1225387A
(en)

*

1983-11-10
1987-08-11
David E.W. Vaughan
Process for preparing type l zeolites by nucleation technique

DE3402842A1
(en)

*

1984-01-27
1985-08-08
Süd-Chemie AG, 8000 München

METHOD FOR PRODUCING CRYSTALLINE ZEOLITHIC ALUMOSILICATES

US4585637A
(en)

*

1984-06-26
1986-04-29
Mobil Oil Corporation
Synthesis of crystalline silicate ZSM-12

US4689207A
(en)

*

1985-03-06
1987-08-25
Chevron Research Company
Process for the preparation of crystalline microporous organosilicates using magadiite as a silica source

US4676958A
(en)

*

1985-03-06
1987-06-30
Chevron Research Company
Preparation of crystalline zeolites using magadiite

FR2582234B1
(en)

*

1985-05-23
1993-03-12
Centre Nat Rech Scient

OMEGA TYPE ZEOLITE WITH HIGH THERMAL STABILITY, PREPARATION METHOD THEREOF AND USE THEREOF AS CATALYST

US4840779A
(en)

*

1985-07-08
1989-06-20
Uop
Crystalline zeolite LZ-202 and process for preparing same

US4931266A
(en)

*

1986-10-22
1990-06-05
Union Oil Company Of California
Crystalline galliosilicate with the erionite-type structure

US5064793A
(en)

*

1986-10-22
1991-11-12
Union Oil Company Of California
Catalyst composition containing a crystalline galliosilicate having the erionite-type structure

JPS63162520A
(en)

*

1986-12-26
1988-07-06
Tosoh Corp
Production of synthetic mazzite

US4857288A
(en)

*

1987-05-15
1989-08-15
Uop
Zeolite LZ-135 and process for preparing same

US5110573A
(en)

*

1990-08-16
1992-05-05
Mobil Oil Corporation
Silica-alumina-organic amine product, its synthesis and use in zeolite production

CA2093303C
(en)

*

1992-04-09
1998-11-24
Abraham Araya
Aluminosilicates

US5330736A
(en)

*

1992-12-07
1994-07-19
W. R. Grace & Co.-Conn.
Zeolite L synthesis and resulting product

DE69605172T2
(en)

*

1995-07-10
2000-08-24
Exxon Chemical Patents Inc

ZEOLITES AND METHOD FOR THEIR PRODUCTION

CN1043749C
(en)

*

1995-10-06
1999-06-23
中国石油化工总公司
Zeolite with MOR structure and its composition

FR3009300B1
(en)

2013-08-05
2022-11-25
Ceca Sa

ZEOLITHS WITH HIERARCHIZED POROSITY

FR3010071B1
(en)

2013-09-02
2015-08-21
Ceca Sa

ZEOLITHES HIERARCHISED POROSITY

FR3025789B1
(en)

2014-09-12
2018-04-20
Arkema France

ZEOLITH NANOCRYSTAL AGGREGATES

US20170158520A1
(en)

*

2015-12-04
2017-06-08
Chevron U.S.A. Inc.
Synthesis of aluminosilicate zeolites having the offretite structure

CN105668585B
(en)

*

2016-01-04
2018-01-16
北京科技大学
The method that zeolite L is prepared using directed agents

CN108495815B
(en)

*

2016-04-12
2021-08-17
雪佛龙美国公司
Synthesis of molecular sieve SSZ-98

CN107473238B
(en)

*

2016-06-08
2019-11-01
中国石油化工股份有限公司
A kind of KL molecular sieve and its preparation method and application

CN109205637B
(en)

*

2017-07-05
2021-10-08
中国石油化工股份有限公司
SAPO-35 molecular sieve, and preparation method and application thereof

US20210380425A1
(en)

*

2018-11-01
2021-12-09
Exxonmobil Research And Engineering Company
Highly Siliceous Form of Zeolite RHO

Family Cites Families (7)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

US3306922A
(en)

*

1961-03-22
1967-02-28
Union Carbide Corp
Molecular sieve adsorbents

US3314752A
(en)

*

1961-08-30
1967-04-18
Mobil Oil Corp
Synthetic zeolite

NL289199A
(en)

*

1962-02-21

US3355246A
(en)

*

1966-07-18
1967-11-28
Mobil Oil Corp
Crystalline zeolite zk-21

US3578398A
(en)

*

1968-04-01
1971-05-11
Mobil Oil Corp
Synthetic crystalline zeolite and preparation thereof

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*

1969-10-10
1972-11-14
Mobil Oil Corp
Crystalline zeolite zsm-5 and method of preparing the same

US3808326A
(en)

*

1971-03-19
1974-04-30
Grace W R & Co
Preparation of zeolites

1974

1974-03-20
US
US05/452,734
patent/US3947482A/en
not_active
Expired – Lifetime

1974-10-24
CA
CA212,174A
patent/CA1038850A/en
not_active
Expired

1975

1975-03-19
JP
JP50032491A
patent/JPS5813492B2/en
not_active
Expired

1975-03-19
GB
GB11464/75A
patent/GB1501461A/en
not_active
Expired

1975-03-19
DE
DE19752511975
patent/DE2511975A1/en
not_active
Withdrawn

Cited By (4)

* Cited by examiner, † Cited by third party

Publication number
Priority date
Publication date
Assignee
Title

CN104071802A
(en)

*

2014-07-03
2014-10-01
太原理工大学
Preparation method for hierarchical pore low-silicate zeolite

CN104071802B
(en)

*

2014-07-03
2015-12-02
太原理工大学
The preparation method of the low silicone zeolite of a kind of multi-stage porous

CN106542539A
(en)

*

2016-10-25
2017-03-29
浙江大学
In the method that polyquaternary ammonium salt template synthesizes 23 zeolite molecular sieves of macropore EMM

CN108862305A
(en)

*

2018-07-17
2018-11-23
武汉科技大学
A method of acid resistance OFF type adsorbent of molecular sieve is synthesized using Coaseries kaolin

Also Published As

Publication number
Publication date

DE2511975A1
(en)

1975-09-25

US3947482A
(en)

1976-03-30

JPS50131897A
(en)

1975-10-18

JPS5813492B2
(en)

1983-03-14

CA1038850A
(en)

1978-09-19

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Legal Events

Date
Code
Title
Description

1978-06-28
PS
Patent sealed [section 19, patents act 1949]

1987-11-11
PCNP
Patent ceased through non-payment of renewal fee

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